C₂₇H₃₆O₇

Base Information

Chemical Name:C₂₇H₃₆O₇
CAS No.:1362110-62-0
Molecular Formula:C₂₇H₃₆O₇
Molecular Weight:472.579
Hs Code.:

C<sub>27</sub>H<sub>36</sub>O<sub>7</sub>

Synonyms:C₂₇H₃₆O₇

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Chemical Property of C₂₇H₃₆O₇

Chemical Property:

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Technology Process of C₂₇H₃₆O₇

There total 15 articles about C₂₇H₃₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1362110-37-9
C₂₅H₃₂O₆

: 107-30-2
chloromethyl methyl ether

: 1362110-62-0
C₂₇H₃₆O₇

Guidance literature:: With N-ethyl-N,N-diisopropylamine; sodium iodide; In 1,2-dimethoxyethane; for 24h; Reflux;
DOI:10.1021/ol300390k

Reference yield:

: 1362110-27-7
C₃₂H₄₆O₃Si

: 1362110-62-0
C₂₇H₃₆O₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

3.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

5.2: brine

6.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

7.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

9.1: ammonia / methanol; water / 6 h / 66 °C

9.2: 0 °C / pH 2

10.1: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

11.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 100 °C / Inert atmosphere

12.1: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / 24 h / Reflux

With pyridine; 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 6.1: Sharpless epoxidation;
DOI:10.1021/ol300390k

Reference yield:

: C₃₉H₅₁ClO₆Si

: 1362110-62-0
C₂₇H₃₆O₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

2.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

4.2: brine

5.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

8.1: ammonia / methanol; water / 6 h / 66 °C

8.2: 0 °C / pH 2

9.1: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

10.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 100 °C / Inert atmosphere

11.1: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / 24 h / Reflux

With pyridine; 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 5.1: Sharpless epoxidation;
DOI:10.1021/ol300390k