phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside
CAS No.:371123-28-3
Molecular Formula:C₂₂H₂₂Cl₃NO₆S
Molecular Weight:534.845
Hs Code.:

Synonyms:phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 188583-24-6
phenyl 2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

: 371123-28-3
phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In acetonitrile; at 20 ℃; regioselective reaction; Inert atmosphere; Sonication;
DOI:10.1002/adsc.201100228

Reference yield: 78.0%

: 371123-28-3
phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

: 86520-63-0
2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate

: phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-4,6-O-benzylidene-2-deoxy-1-thio-2-[(2,2,2-trichloroethoxy)carbonyl]amino-β-D-glucopyranoside

Guidance literature:: With 1-(n-butyl)-3-methylimidazolium triflate; In dichloromethane; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tetlet.2008.11.042

Reference yield:

: 371123-28-3
phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

: 86520-63-0
2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate

: phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-4,6-O-benzylidene-2-deoxy-1-thio-2-[(2,2,2-trichloroethoxy)carbonyl]amino-β-D-glucopyranoside

: 2872-72-2
phenyl-2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Guidance literature:: phenyl 2-[(2,2,2-trichloroethoxy)carbonyl]amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside; 2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate; With 1H-imidazole; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1002/adsc.201100228