C₅₅H₆₂O₁₆

Base Information

Chemical Name:C₅₅H₆₂O₁₆
CAS No.:1018988-56-1
Molecular Formula:C₅₅H₆₂O₁₆
Molecular Weight:979.088
Hs Code.:

C<sub>55</sub>H<sub>62</sub>O<sub>16</sub>

Synonyms:C₅₅H₆₂O₁₆

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Chemical Property of C₅₅H₆₂O₁₆

Chemical Property:

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Technology Process of C₅₅H₆₂O₁₆

There total 25 articles about C₅₅H₆₂O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 117122-29-9
C₂₈H₄₀O₉

: 161007-95-0
2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyltrichloroacetimidate

: 1018988-56-1
C₅₅H₆₂O₁₆

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.200704959

Reference yield:

: 1018988-60-7
C₅₈H₇₈O₇Si₃

: 1018988-56-1
C₅₅H₆₂O₁₆

Guidance literature:: Multi-step reaction with 22 steps

1.1: 2,6-di-tert-butyl-4-methylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / -40 - -30 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 13 °C / Inert atmosphere

4.1: lithium borohydride / tetrahydrofuran / Inert atmosphere; Reflux

4.2: 4 h / 20 °C / Inert atmosphere

5.1: lithium borohydride / tetrahydrofuran / 26.5 h / 20 °C / Inert atmosphere; Reflux

5.2: 4 h / 20 °C / Inert atmosphere

6.1: water; acetic acid / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

7.1: dmap / pyridine; dichloromethane / 24 h / 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

9.1: peracetic acid; mercury(II) diacetate; acetic acid / 4 h / 20 °C / Inert atmosphere

10.1: 1H-imidazole / dichloromethane / 4 h / 0 °C / Inert atmosphere

11.1: dmap / pyridine; dichloromethane / 0 - 40 °C / Inert atmosphere

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

13.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

14.1: Wilkinson's catalyst; triphenylphosphine; isopropyl alcohol / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

15.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 5 h / 20 °C / Inert atmosphere

16.1: di(n-butyl)tin oxide / benzene / 16 h / Reflux; Inert atmosphere

16.2: 0.17 h / 20 °C / Inert atmosphere; Molecular sieve

17.1: triethylamine / benzene / 24 h / 20 °C / Inert atmosphere

18.1: sodium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

19.1: hydrogenchloride / 4 h / 20 °C / Inert atmosphere

20.1: pyridine; dmap / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

21.1: sodium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

22.1: dichloromethane / 0.17 h / 20 °C / Molecular sieve; Inert atmosphere

22.2: Inert atmosphere

22.3: 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogenchloride; peracetic acid; dmap; sodium tetrahydroborate; Wilkinson's catalyst; osmium(VIII) oxide; lithium borohydride; 2,6-di-tert-butyl-4-methylpyridine; mercury(II) diacetate; tetrabutyl ammonium fluoride; water; di(n-butyl)tin oxide; sodium hydrogencarbonate; sodium carbonate; Dess-Martin periodane; acetic acid; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; isopropyl alcohol; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; benzene; 2.1: Luche reduction / 9.1: Tamao oxidation;
DOI:10.1002/asia.200800429

Reference yield:

: 1018988-59-4
C₅₂H₆₆O₇Si₂

: 1018988-56-1
C₅₅H₆₂O₁₆

Guidance literature:: Multi-step reaction with 25 steps

1.1: sodium tetrahydroborate / ethanol / 2 h / -78 °C / Inert atmosphere

2.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 39 h / 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: 2,6-di-tert-butyl-4-methylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile / 20 °C / Inert atmosphere

5.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / -40 - -30 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 13 °C / Inert atmosphere

7.1: lithium borohydride / tetrahydrofuran / Inert atmosphere; Reflux

7.2: 4 h / 20 °C / Inert atmosphere

8.1: lithium borohydride / tetrahydrofuran / 26.5 h / 20 °C / Inert atmosphere; Reflux

8.2: 4 h / 20 °C / Inert atmosphere

9.1: water; acetic acid / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

10.1: dmap / pyridine; dichloromethane / 24 h / 20 °C / Inert atmosphere

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

12.1: peracetic acid; mercury(II) diacetate; acetic acid / 4 h / 20 °C / Inert atmosphere

13.1: 1H-imidazole / dichloromethane / 4 h / 0 °C / Inert atmosphere

14.1: dmap / pyridine; dichloromethane / 0 - 40 °C / Inert atmosphere

15.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

16.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

17.1: Wilkinson's catalyst; triphenylphosphine; isopropyl alcohol / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

18.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 5 h / 20 °C / Inert atmosphere

19.1: di(n-butyl)tin oxide / benzene / 16 h / Reflux; Inert atmosphere

19.2: 0.17 h / 20 °C / Inert atmosphere; Molecular sieve

20.1: triethylamine / benzene / 24 h / 20 °C / Inert atmosphere

21.1: sodium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

22.1: hydrogenchloride / 4 h / 20 °C / Inert atmosphere

23.1: pyridine; dmap / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

24.1: sodium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

25.1: dichloromethane / 0.17 h / 20 °C / Molecular sieve; Inert atmosphere

25.2: Inert atmosphere

25.3: 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogenchloride; peracetic acid; dmap; sodium tetrahydroborate; Wilkinson's catalyst; osmium(VIII) oxide; lithium borohydride; 2,6-di-tert-butyl-4-methylpyridine; mercury(II) diacetate; tetrabutyl ammonium fluoride; water; di(n-butyl)tin oxide; sodium hydrogencarbonate; sodium carbonate; Dess-Martin periodane; acetic acid; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; isopropyl alcohol; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; benzene; 5.1: Luche reduction / 12.1: Tamao oxidation;
DOI:10.1002/asia.200800429