N²,N²,N^2',N^2'-Tetrakis-(2,4-dimethoxy-benzyl)-4,4'-bis-dodecyloxy-[5,5']bipyrimidinyl-2,2'-diamine

Base Information

• Chemical Name: N²,N²,N^2',N^2'-Tetrakis-(2,4-dimethoxy-benzyl)-4,4'-bis-dodecyloxy-[5,5']bipyrimidinyl-2,2'-diamine
• CAS No.: 218459-17-7
• Molecular Formula: C₆₈H₉₆N₆O₁₀
• Molecular Weight: 1157.54

Synonyms:N²,N²,N^2',N^2'-Tetrakis-(2,4-dimethoxy-benzyl)-4,4'-bis-dodecyloxy-[5,5']bipyrimidinyl-2,2'-diamine

Chemical Property of N²,N²,N^2',N^2'-Tetrakis-(2,4-dimethoxy-benzyl)-4,4'-bis-dodecyloxy-[5,5']bipyrimidinyl-2,2'-diamine

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Technology Process of N²,N²,N^2',N^2'-Tetrakis-(2,4-dimethoxy-benzyl)-4,4'-bis-dodecyloxy-[5,5']bipyrimidinyl-2,2'-diamine

There total 2 articles about N²,N²,N^2',N^2'-Tetrakis-(2,4-dimethoxy-benzyl)-4,4'-bis-dodecyloxy-[5,5']bipyrimidinyl-2,2'-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-dodecyl alcohol (112-53-8) + 4,4'-Dichloro-N2,N2,N2',N2'-tetrakis-(2,4-dimethoxy-benzyl)-[5,5']bipyrimidinyl-2,2'-diamine (218459-11-1) → N2,N2,N2',N2'-Tetrakis-(2,4-dimethoxy-benzyl)-4,4'-bis-dodecyloxy-[5,5']bipyrimidinyl-2,2'-diamine (218459-17-7)

Guidance literature:

With sodium; In toluene; at 120 ℃; for 24h;

DOI:10.1002/(SICI)1522-2675(19981111)81:11<1921::AID-HLCA1921>3.0.CO;2-7

Reference yield:

2,2',4,4'-tetrachloro-5,5'-bipyrimidine (53734-80-8) → N2,N2,N2',N2'-Tetrakis-(2,4-dimethoxy-benzyl)-4,4'-bis-dodecyloxy-[5,5']bipyrimidinyl-2,2'-diamine (218459-17-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / Et₃N / toluene / 2.5 h / Heating

2: 92 percent / Na / toluene / 24 h / 120 °C

With sodium; triethylamine; In toluene;

DOI:10.1002/(SICI)1522-2675(19981111)81:11<1921::AID-HLCA1921>3.0.CO;2-7

upstream raw materials:

1-dodecyl alcohol

4,4'-Dichloro-N²,N²,N^2',N^2'-tetrakis-(2,4-dimethoxy-benzyl)-[5,5']bipyrimidinyl-2,2'-diamine

2,2',4,4'-tetrachloro-5,5'-bipyrimidine

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