Re₂Cl₆(P(C₆H₅)3)2

Base Information

Chemical Name:Re₂Cl₆(P(C₆H₅)3)2
CAS No.:11087-98-2
Molecular Formula:C₃₆H₃₀Cl₆P₂Re₂
Molecular Weight:1109.71
Hs Code.:

Re<sub>2</sub>Cl<sub>6</sub>(P(C<sub>6</sub>H<sub>5</sub>)3)2

Synonyms:Re₂Cl₆(P(C₆H₅)3)2

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Chemical Property of Re₂Cl₆(P(C₆H₅)3)2

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Technology Process of Re₂Cl₆(P(C₆H₅)3)2

There total 2 articles about Re₂Cl₆(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85335-14-4
2(C₆H₅)3PC₃H₅⁽¹⁺⁾*Re₂Cl₈^(2-)=((C₆H₅)3PC₃H₅)2Re₂Cl₈

: 11087-98-2
Re₂Cl₆(P(C₆H₅)3)2

Guidance literature:: With hydrogenchloride; triphenylphosphine; In methanol; under N2, PPh3 was dissolved in MeOH containing concd. HCl, treated with Re-complex, stirred for 30 min; filtered, washed with MeOH, dried under vac.; identified by spectroscopic properties;

Reference yield:

: 83511-36-8
2(C₆H₅)3PH⁽¹⁺⁾*Re₂Cl₈^(2-)=((C₆H₅)3PH)2Re₂Cl₈

: 11087-98-2
Re₂Cl₆(P(C₆H₅)3)2

Guidance literature:: In methanol; under N2, Re-complex was dissolved in MeOH;

Reference yield: 87.0%

: 16940-66-2
sodium tetrahydroborate

: 11087-98-2
Re₂Cl₆(P(C₆H₅)3)2

: Re2(μ-H)4H4(triphenylphosphine)4

Guidance literature:: With triphenylphosphine; In ethanol; byproducts: sodium chloride; under N2, suspn. of Re-complex and PPh3 (molar ratio 1:2.15) in abs. EtOH was stirred for 30 min at room temp., solid NaBH4 was added, stirred for 15 min, refluxed for 15 min; filtered warm, ppt. washed with MeOH, then with H2O-EtOH, EtOH and Et2O, vac. dried, suspn. in CH3CN refluxed; elem. anal.;