2,2,2-Trichloro-acetimidic acid (2S,3S)-3-benzyloxymethyl-oxiranylmethyl ester

Base Information

Chemical Name:2,2,2-Trichloro-acetimidic acid (2S,3S)-3-benzyloxymethyl-oxiranylmethyl ester
CAS No.:188476-46-2
Molecular Formula:C₁₃H₁₄Cl₃NO₃
Molecular Weight:338.618
Hs Code.:

Synonyms:2,2,2-Trichloro-acetimidic acid (2S,3S)-3-benzyloxymethyl-oxiranylmethyl ester

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Chemical Property of 2,2,2-Trichloro-acetimidic acid (2S,3S)-3-benzyloxymethyl-oxiranylmethyl ester

Chemical Property:

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Technology Process of 2,2,2-Trichloro-acetimidic acid (2S,3S)-3-benzyloxymethyl-oxiranylmethyl ester

There total 1 articles about 2,2,2-Trichloro-acetimidic acid (2S,3S)-3-benzyloxymethyl-oxiranylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78469-85-9,78513-07-2,78513-15-2,84621-89-6,87172-27-8,95672-91-6,98048-62-5,98048-63-6,78513-12-9
(2S,3S)-4-benzyloxy-2,3-epoxy-1-butanol

: 545-06-2
trichloroacetonitrile

: 188476-46-2
2,2,2-Trichloro-acetimidic acid (2S,3S)-3-benzyloxymethyl-oxiranylmethyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃;
DOI:10.1021/jo9618278

Reference yield: 60.0%

: 188476-46-2
2,2,2-Trichloro-acetimidic acid (2S,3S)-3-benzyloxymethyl-oxiranylmethyl ester

: (R)-2-Benzyloxy-1-((R)-2-trichloromethyl-4,5-dihydro-oxazol-4-yl)-ethanol

Guidance literature:: With diethylaluminium chloride; In hexane; dichloromethane; at 20 ℃; for 0.0833333h;
DOI:10.1016/S0040-4020(02)00305-8

Reference yield:

: 188476-46-2
2,2,2-Trichloro-acetimidic acid (2S,3S)-3-benzyloxymethyl-oxiranylmethyl ester

: (R)-2-Benzyloxy-1-((R)-2-trichloromethyl-4,5-dihydro-oxazol-4-yl)-ethanol

: N-((1R,2R)-3-Benzyloxy-2-hydroxy-1-hydroxymethyl-propyl)-2,2,2-trichloro-acetamide

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -23 ℃; Yield given. Yields of byproduct given;
DOI:10.1021/jo9618278