2-methoxyethyl 2-(4-mesylaminophenyl)-5⁽⁶⁾-benzimidazolecarboximidate dihydrochloride

Base Information

• Chemical Name: 2-methoxyethyl 2-(4-mesylaminophenyl)-5⁽⁶⁾-benzimidazolecarboximidate dihydrochloride
• CAS No.: 136491-93-5
• Molecular Formula: C₁₈H₂₀N₄O₄S*2ClH
• Molecular Weight: 461.369

Synonyms:2-methoxyethyl 2-(4-mesylaminophenyl)-5⁽⁶⁾-benzimidazolecarboximidate dihydrochloride

Chemical Property of 2-methoxyethyl 2-(4-mesylaminophenyl)-5⁽⁶⁾-benzimidazolecarboximidate dihydrochloride

Chemical Property:

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Technology Process of 2-methoxyethyl 2-(4-mesylaminophenyl)-5⁽⁶⁾-benzimidazolecarboximidate dihydrochloride

There total 3 articles about 2-methoxyethyl 2-(4-mesylaminophenyl)-5⁽⁶⁾-benzimidazolecarboximidate dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-methoxy-ethanol (109-86-4,95507-80-5) + 2-(4-mesylaminophenyl)-5(6)-benzimidazolecarbonitrile (136491-89-9) → 2-methoxyethyl 2-(4-mesylaminophenyl)-5(6)-benzimidazolecarboximidate dihydrochloride (136491-93-5)

Guidance literature:

With hydrogenchloride; at 0 ℃; for 48h;

Reference yield:

4-cyano-1,2-phenylenediamine (17626-40-3) → 2-methoxyethyl 2-(4-mesylaminophenyl)-5(6)-benzimidazolecarboximidate dihydrochloride (136491-93-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / acetic acid / 5 h / Heating

2: 94 percent / HCl (gas) / 48 h / 0 °C

With hydrogenchloride; In acetic acid;

Reference yield:

2-methoxyethyl 4-mesylaminobenzimidate hydrochloride (106307-03-3) → 2-methoxyethyl 2-(4-mesylaminophenyl)-5(6)-benzimidazolecarboximidate dihydrochloride (136491-93-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / acetic acid / 5 h / Heating

2: 94 percent / HCl (gas) / 48 h / 0 °C

With hydrogenchloride; In acetic acid;

upstream raw materials:

2-methoxy-ethanol

2-(4-mesylaminophenyl)-5⁽⁶⁾-benzimidazolecarbonitrile

4-cyano-1,2-phenylenediamine

2-methoxyethyl 4-mesylaminobenzimidate hydrochloride

Downstream raw materials:

2'-(4-Methanesulfonylamino-phenyl)-1H,1'H-[2,5']bibenzoimidazolyl-5-carboxylic acid (3-dimethylamino-propyl)-amide; hydrochloride

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