[(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside

Base Information

Chemical Name:[(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside
CAS No.:1026073-72-2
Molecular Formula:C₃₄H₄₂O₆
Molecular Weight:546.704
Hs Code.:

Synonyms:[(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside

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Chemical Property of [(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside

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Technology Process of [(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside

There total 2 articles about [(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1026073-68-6
C₅₃H₅₆O₆

: 1026073-72-2
[(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside

Guidance literature:: C₅₃H₅₆O₆; With triethylsilane; zinc dibromide; In dichloromethane; for 8h;

With water; sodium hydrogencarbonate; In dichloromethane;

Reference yield:

: 169532-17-6,116391-11-8
ethyl 2,3,4-tri-O-benzyl-1-thio-α/β-L-fucopyranoside

: 1026073-72-2
[(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: bromine / dichloromethane / 0.83 h / 0 °C

1.2: 0.33 h / 0 °C

1.3: 16 h / 20 °C / Molecular sieve

2.1: triethylsilane; zinc dibromide / dichloromethane / 8 h / 20 °C

With triethylsilane; bromine; zinc dibromide; In dichloromethane;
DOI:10.1002/chem.201102884

Reference yield: 79.0%

: 1026073-72-2
[(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside

: ethyl 6-O-benzyl-2,3,4-tri-O-benzoyl-thio-β-D-galactopyranoside

: C₆₈H₇₀O₁₄

Guidance literature:: [(1R,2R,3S)-1-hydroxy-3-methylcyclohex-2-yl] 2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranoside; ethyl 6-O-benzyl-2,3,4-tri-O-benzoyl-thio-β-D-galactopyranoside; In dichloromethane; at 20 ℃; for 4h; Molecular sieve;

With DMTST; In dichloromethane; at 20 ℃; for 72h; Molecular sieve;