2-(aminocarbonyl)-2-[(4-methylphenyl)methyl]hydrazinecarboxylic acid, 1,1-dimethylethyl ester

Base Information

Chemical Name:2-(aminocarbonyl)-2-[(4-methylphenyl)methyl]hydrazinecarboxylic acid, 1,1-dimethylethyl ester
CAS No.:425675-43-0
Molecular Formula:C₁₄H₂₁N₃O₃
Molecular Weight:279.339
Hs Code.:

Synonyms:2-(aminocarbonyl)-2-[(4-methylphenyl)methyl]hydrazinecarboxylic acid, 1,1-dimethylethyl ester

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Chemical Property of 2-(aminocarbonyl)-2-[(4-methylphenyl)methyl]hydrazinecarboxylic acid, 1,1-dimethylethyl ester

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Technology Process of 2-(aminocarbonyl)-2-[(4-methylphenyl)methyl]hydrazinecarboxylic acid, 1,1-dimethylethyl ester

There total 2 articles about 2-(aminocarbonyl)-2-[(4-methylphenyl)methyl]hydrazinecarboxylic acid, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1118-02-1
trimethylsilyl isocyanate

: 162739-90-4
2-[(4-methylphenyl)methyl]hydrazinecarboxylic acid 1,1-dimethylethyl ester

: 425675-43-0
2-(aminocarbonyl)-2-[(4-methylphenyl)methyl]hydrazinecarboxylic acid, 1,1-dimethylethyl ester

Guidance literature:: In isopropyl alcohol; at 20 ℃; for 16h; Large scale;
DOI:10.1021/op700040v

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 425675-43-0
2-(aminocarbonyl)-2-[(4-methylphenyl)methyl]hydrazinecarboxylic acid, 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: isopropyl alcohol / 1 h / 50 °C / Autoclave; Large scale

2: platinum on carbon; hydrogen / isopropyl alcohol; water / 8 h / 50 °C / 3345.86 Torr / Autoclave; Large scale

3: isopropyl alcohol / 16 h / 20 °C / Large scale

With platinum on carbon; hydrogen; In water; isopropyl alcohol;
DOI:10.1021/op700040v