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Technology Process of 2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone

2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone

Base Information
  • Chemical Name:2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone
  • CAS No.:1027097-11-5
  • Molecular Formula:C24H37ClN2O4Si
  • Molecular Weight:487.06
  • Hs Code.:
2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d<sub>4</sub>-ethoxy-d<sub>2</sub>-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone

Synonyms:2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone

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Chemical Property of 2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone
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Technology Process of 2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone

There total 1 articles about 2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

{4-[2-(tert-butyldimethylsilanyloxy)-d<sub>4</sub>-ethoxy-d<sub>2</sub>-methyl]phenyl}methanol
1027097-09-1

{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]phenyl}methanol

2-tert-butyl-4-chloro-5-hydroxy-3(2H)-pyridazinone
88093-48-5

2-tert-butyl-4-chloro-5-hydroxy-3(2H)-pyridazinone

2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d<sub>4</sub>-ethoxy-d<sub>2</sub>-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone
1027097-11-5

2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone

Guidance literature:
With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/jm701443n

Reference yield:

2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d<sub>4</sub>-ethoxy-d<sub>2</sub>-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone
1027097-11-5

2-tert-butyl-5-{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]benzyloxy}-4-chloro-3-(2H)-pyridazinone

2-tert-butyl-4-chloro-5-[4-(2-hydroxy-d<sub>4</sub>-ethoxy-d<sub>2</sub>-methyl)benzyloxy]-3-(2H)-pyridazinone
1027097-14-8

2-tert-butyl-4-chloro-5-[4-(2-hydroxy-d4-ethoxy-d2-methyl)benzyloxy]-3-(2H)-pyridazinone

Guidance literature:
With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/jm701443n
upstream raw materials:

{4-[2-(tert-butyldimethylsilanyloxy)-d4-ethoxy-d2-methyl]phenyl}methanol

2-tert-butyl-4-chloro-5-hydroxy-3(2H)-pyridazinone

Downstream raw materials:

2-tert-butyl-4-chloro-5-[4-(2-hydroxy-d4-ethoxy-d2-methyl)benzyloxy]-3-(2H)-pyridazinone

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