N-(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-N'-(2-{2-[(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-amino]-ethylamino}-ethyl)-ethane-1,2-diamine

Base Information

Chemical Name:N-(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-N'-(2-{2-[(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-amino]-ethylamino}-ethyl)-ethane-1,2-diamine
CAS No.:325140-37-2
Molecular Formula:C₃₈H₅₀N₄
Molecular Weight:562.842
Hs Code.:

Synonyms:N-(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-N'-(2-{2-[(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-amino]-ethylamino}-ethyl)-ethane-1,2-diamine

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Chemical Property of N-(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-N'-(2-{2-[(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-amino]-ethylamino}-ethyl)-ethane-1,2-diamine

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Technology Process of N-(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-N'-(2-{2-[(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-amino]-ethylamino}-ethyl)-ethane-1,2-diamine

There total 4 articles about N-(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-N'-(2-{2-[(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-amino]-ethylamino}-ethyl)-ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 325140-36-1
C₃₈H₄₆N₄O₂

: 325140-37-2
N-(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-N'-(2-{2-[(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-amino]-ethylamino}-ethyl)-ethane-1,2-diamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; for 2h; Heating;
DOI:10.1002/anie.200502245

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 325140-37-2
N-(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-N'-(2-{2-[(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-amino]-ethylamino}-ethyl)-ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: 60.2 percent / triphenylphosphine; sodium carbonate; palladium(II) acetate / 1,2-dimethoxy-ethane; propan-2-ol; H₂O / Heating

2: 82.5 percent / 1-hydroxybenzotriazole; 2-(dimethylamino)isopropyl chloride hydrochloride / CH₂Cl₂ / 20 °C

3: LiAlH₄ / diethyl ether; tetrahydrofuran / 2 h / Heating

With lithium aluminium tetrahydride; palladium diacetate; (2-chloropropyl)dimethylamine hydrochloride; sodium carbonate; benzotriazol-1-ol; triphenylphosphine; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; isopropyl alcohol;
DOI:10.1002/anie.200502245

Reference yield:

: 66818-63-1
4-(2,4,6-trimethylphenyl)benzoic acid

: 325140-37-2
N-(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-N'-(2-{2-[(2',4',6'-trimethyl-biphenyl-4-ylmethyl)-amino]-ethylamino}-ethyl)-ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 82.5 percent / 1-hydroxybenzotriazole; 2-(dimethylamino)isopropyl chloride hydrochloride / CH₂Cl₂ / 20 °C

2: LiAlH₄ / diethyl ether; tetrahydrofuran / 2 h / Heating

With lithium aluminium tetrahydride; (2-chloropropyl)dimethylamine hydrochloride; benzotriazol-1-ol; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/anie.200502245