C₃₂H₄₈N₇O₅PSi

Base Information

• Chemical Name: C₃₂H₄₈N₇O₅PSi
• CAS No.: 1435880-61-7
• Molecular Formula: C₃₂H₄₈N₇O₅PSi
• Molecular Weight: 669.836
• Mol file: 1435880-61-7.mol

Synonyms:C₃₂H₄₈N₇O₅PSi

Chemical Property of C₃₂H₄₈N₇O₅PSi

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₂H₄₈N₇O₅PSi

There total 1 articles about C₃₂H₄₈N₇O₅PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) + N6-benzoyl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine (51549-39-4) → C32H48N7O5PSi (1435880-61-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 4h;

DOI:10.1016/j.tetlet.2013.04.043

Reference yield: 18.0%

C32H48N7O5PSi (1435880-61-7) + tetrabutyl ammonium fluoride (429-41-4) + tetrakis(ω-hydroxybutyl)methylene-bridged cavitand (214276-10-5) → C112H116N12O40P4(4-)*4C16H36N(1+)

Guidance literature:

C₃₂H₄₈N₇O₅PSi; tetrakis(ω-hydroxybutyl)methylene-bridged cavitand; With 5-(ethylthio)-1H-tetrazole; In dichloromethane; for 3h; Inert atmosphere;

With pyridine; iodine; In dichloromethane; water; at 0 ℃; for 0.0833333h; Inert atmosphere;

tetrabutyl ammonium fluoride; Further stages;

DOI:10.1016/j.tetlet.2013.04.043

upstream raw materials:

2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

N⁶-benzoyl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine