methyl 6-(3-methoxyphenyl)sulfanyl-2,4-dimethyl-3-(2-phenyldiazen-1-yl)benzoate

Base Information

Chemical Name:methyl 6-(3-methoxyphenyl)sulfanyl-2,4-dimethyl-3-(2-phenyldiazen-1-yl)benzoate
CAS No.:1520853-92-2
Molecular Formula:C₂₃H₂₂N₂O₃S
Molecular Weight:406.505
Hs Code.:

Synonyms:methyl 6-(3-methoxyphenyl)sulfanyl-2,4-dimethyl-3-(2-phenyldiazen-1-yl)benzoate

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Chemical Property of methyl 6-(3-methoxyphenyl)sulfanyl-2,4-dimethyl-3-(2-phenyldiazen-1-yl)benzoate

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Technology Process of methyl 6-(3-methoxyphenyl)sulfanyl-2,4-dimethyl-3-(2-phenyldiazen-1-yl)benzoate

There total 4 articles about methyl 6-(3-methoxyphenyl)sulfanyl-2,4-dimethyl-3-(2-phenyldiazen-1-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1023305-06-7
C₁₅H₂₂O₃SSi

: 1020261-65-7
3-(phenyldiazenyl)-4-(trimethylsilyloxy)pent-3-en-2-one

: 1520853-92-2
methyl 6-(3-methoxyphenyl)sulfanyl-2,4-dimethyl-3-(2-phenyldiazen-1-yl)benzoate

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -78 - 20 ℃; for 20h; Inert atmosphere;
DOI:10.1080/10426507.2013.818999

Reference yield:

: acetylacetone phenylhydrazone

: 1520853-92-2
methyl 6-(3-methoxyphenyl)sulfanyl-2,4-dimethyl-3-(2-phenyldiazen-1-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / pentane / 25 °C / Inert atmosphere

2: titanium tetrachloride / dichloromethane / 20 h / -78 - 20 °C / Inert atmosphere

With titanium tetrachloride; triethylamine; In dichloromethane; pentane;
DOI:10.1080/10426507.2013.818999

Reference yield:

: 62-53-3
aniline

: 1520853-92-2
methyl 6-(3-methoxyphenyl)sulfanyl-2,4-dimethyl-3-(2-phenyldiazen-1-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; hydrogenchloride / 0.17 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 °C / Inert atmosphere

2.1: triethylamine / pentane / 25 °C / Inert atmosphere

3.1: titanium tetrachloride / dichloromethane / 20 h / -78 - 20 °C / Inert atmosphere

With hydrogenchloride; titanium tetrachloride; triethylamine; sodium nitrite; In dichloromethane; pentane;
DOI:10.1080/10426507.2013.818999