C₂₇H₂₇N₇O

Base Information

Chemical Name:C₂₇H₂₇N₇O
CAS No.:1228633-45-1
Molecular Formula:C₂₇H₂₇N₇O
Molecular Weight:465.558
Hs Code.:

C<sub>27</sub>H<sub>27</sub>N<sub>7</sub>O

Synonyms:C₂₇H₂₇N₇O

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Chemical Property of C₂₇H₂₇N₇O

Chemical Property:

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Technology Process of C₂₇H₂₇N₇O

There total 7 articles about C₂₇H₂₇N₇O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228554-48-0
C₃₇H₄₃N₇O₅

: 1228633-45-1
C₂₇H₂₇N₇O

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 3h;

Reference yield:

: 69610-40-8
N-(tert-butoxycarbonyl)-L-prolinol

: 1228633-45-1
C₂₇H₂₇N₇O

Guidance literature:: Multi-step reaction with 6 steps

1.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / Inert atmosphere; Cooling with ice

2.1: ammonium hydroxide / water; methanol / 19 h / 25 °C

3.1: N-Bromosuccinimide / tetrahydrofuran / 25 °C / Inert atmosphere

4.1: sodium sulfite / ethanol; water / Reflux

5.1: sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; tetrahydrofuran / 100 °C / Inert atmosphere

6.1: hydrogenchloride / methanol / 3 h / 25 °C

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium hydroxide; N-Bromosuccinimide; oxalyl dichloride; sodium carbonate; dimethyl sulfoxide; sodium sulfite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 5.1: |Suzuki Coupling;

Reference yield:

: 40925-68-6
2-amino-4-bromo-phenol

: 1228633-45-1
C₂₇H₂₇N₇O

Guidance literature:: Multi-step reaction with 4 steps

1: Polyphosphoric acid / 1.5 h / 140 °C

2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 100 °C / Inert atmosphere

3: sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; tetrahydrofuran / 100 °C / Inert atmosphere

4: hydrogenchloride / methanol / 3 h / 25 °C

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; sodium carbonate; In tetrahydrofuran; 1,4-dioxane; methanol; water; 3: |Suzuki Coupling;