Technology Process of C19H20O6
There total 14 articles about C19H20O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: AD-mix-β; water / Inert atmosphere
2: triethylamine / Inert atmosphere
3: sodium hydride / Inert atmosphere
4: triethylsilane; dichloro-acetic acid / Inert atmosphere
5: oxalyl dichloride; dimethyl sulfoxide / Inert atmosphere
6: sodium dihydrogenphosphate; sodium chlorite / Inert atmosphere
7: methanol; diethyl ether; toluene / 1 h / 20 °C / Inert atmosphere
With
triethylsilane; dichloro-acetic acid; sodium chlorite; sodium dihydrogenphosphate; oxalyl dichloride; AD-mix-β; water; sodium hydride; dimethyl sulfoxide; triethylamine;
In
methanol; diethyl ether; toluene;
1: Sharpless dihydroxylation / 5: Swern oxidation / 6: Lindgren-Kraus oxidation;
DOI:10.1016/j.tet.2011.04.094
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / Inert atmosphere
2: sodium hydride / Inert atmosphere
3: triethylsilane; dichloro-acetic acid / Inert atmosphere
4: oxalyl dichloride; dimethyl sulfoxide / Inert atmosphere
5: sodium dihydrogenphosphate; sodium chlorite / Inert atmosphere
6: methanol; diethyl ether; toluene / 1 h / 20 °C / Inert atmosphere
With
triethylsilane; dichloro-acetic acid; sodium chlorite; sodium dihydrogenphosphate; oxalyl dichloride; sodium hydride; dimethyl sulfoxide; triethylamine;
In
methanol; diethyl ether; toluene;
4: Swern oxidation / 5: Lindgren-Kraus oxidation;
DOI:10.1016/j.tet.2011.04.094
