Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Base Information

• Chemical Name: Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester
• CAS No.: 934559-18-9
• Molecular Formula: C₆₉H₆₇O₁₆P₃
• Molecular Weight: 1245.2

Synonyms:Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Chemical Property of Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

There total 2 articles about Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

D-1-O-bnzoyl-2,6-di-O-benzyl-myo-inositol (882024-20-6) + Dibenzyl N,N-diisopropylphosphoramidite (108549-23-1) → Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester (934559-18-9)

Guidance literature:

D-1-O-bnzoyl-2,6-di-O-benzyl-myo-inositol; Dibenzyl N,N-diisopropylphosphoramidite; With 1H-tetrazole; In dichloromethane; at 20 ℃; for 0.75h;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2007.01.095

Reference yield:

Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphanyloxy)-cyclohexyl ester → Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester (934559-18-9)

Guidance literature:

With oxidation reagent;

DOI:10.1016/j.tetasy.2005.12.008

Reference yield: 96.0%

Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester (934559-18-9) → (-)-2,6-di-O-benzyl-myo-inositol 3,4,5-tris(dibenzyl phosphate) (160247-11-0)

Guidance literature:

With ethylmagnesium chloride; In tetrahydrofuran; at -42 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2007.01.095

upstream raw materials:

D-1-O-bnzoyl-2,6-di-O-benzyl-myo-inositol

Dibenzyl N,N-diisopropylphosphoramidite

Downstream raw materials:

(-)-2,6-di-O-benzyl-myo-inositol 3,4,5-tris(dibenzyl phosphate)

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 934559-18-9 Benzoic acid (1R,2S,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4,5-tris-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send