Technology Process of C30H42O7
There total 11 articles about C30H42O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 76 percent / aq. NaOH / tetrahydrofuran / 48 h / Heating
2: 93 percent / pyridine / 96 h / 20 °C
3: PBu3; NEt3; HCOOH / Pd(dba)2 / tetrahydrofuran / Heating
4: 67 percent / OsO4; NMMO / tetrahydrofuran; H2O; 2-methyl-propan-2-ol / 144 h / 20 °C
5: 61 percent / DIBALH / CH2Cl2; toluene / 0.5 h
6: 99 percent / sodium periodate / tetrahydrofuran; H2O / 72 h / 20 °C
7: 92 percent / imidazole / dimethylformamide / 5 h / 20 °C
8: 88 percent / NaBH4 / methanol / 0.33 h / 0 °C
9: 57 percent / n-butyllithium / tetrahydrofuran; hexane / 20 h / 20 °C
10: 48 percent / tert-butyl hydroperoxide; palladium(II) acetate / toluene / 72 h / 50 °C
11: 91 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C
With
1H-imidazole; tert.-butylhydroperoxide; sodium hydroxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; formic acid; tributylphosphine; tetrabutyl ammonium fluoride; palladium diacetate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine;
bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O
- Guidance literature:
-
Multi-step reaction with 9 steps
1: PBu3; NEt3; HCOOH / Pd(dba)2 / tetrahydrofuran / Heating
2: 67 percent / OsO4; NMMO / tetrahydrofuran; H2O; 2-methyl-propan-2-ol / 144 h / 20 °C
3: 61 percent / DIBALH / CH2Cl2; toluene / 0.5 h
4: 99 percent / sodium periodate / tetrahydrofuran; H2O / 72 h / 20 °C
5: 92 percent / imidazole / dimethylformamide / 5 h / 20 °C
6: 88 percent / NaBH4 / methanol / 0.33 h / 0 °C
7: 57 percent / n-butyllithium / tetrahydrofuran; hexane / 20 h / 20 °C
8: 48 percent / tert-butyl hydroperoxide; palladium(II) acetate / toluene / 72 h / 50 °C
9: 91 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C
With
1H-imidazole; tert.-butylhydroperoxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; formic acid; tributylphosphine; tetrabutyl ammonium fluoride; palladium diacetate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine;
bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O