methyl 15-(p-iodophenyl)-3(RS)-methylpentadecanoate

Base Information

Chemical Name:methyl 15-(p-iodophenyl)-3(RS)-methylpentadecanoate
CAS No.:88336-93-0
Molecular Formula:C₂₃H₃₇IO₂
Molecular Weight:472.45
Hs Code.:

Synonyms:methyl 15-(p-iodophenyl)-3(RS)-methylpentadecanoate

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Chemical Property of methyl 15-(p-iodophenyl)-3(RS)-methylpentadecanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 15-(p-iodophenyl)-3(RS)-methylpentadecanoate

There total 20 articles about methyl 15-(p-iodophenyl)-3(RS)-methylpentadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2834-05-1
11-bromoundecanoic acid

: 88336-93-0
methyl 15-(p-iodophenyl)-3(RS)-methylpentadecanoate

Guidance literature:: Multi-step reaction with 15 steps

1: SOCl₂ / dimethylformamide / 1 h / 80 °C

2: AlCl₃ / dimethylformamide / 1 h / 90 °C

3: 85 percent / dimethylsulfoxide / 2 h / 80 °C

4: 95 percent / NH₂NH₂*H₂O, KOH / bis-(2-hydroxy-ethyl) ether / 4 h / Heating

5: 95 percent / diethyl ether / 12 h / 0 °C

6: 90 percent / LiAlH₄ / diethyl ether / 4 h / Heating

7: 88 percent / Me₃SiI / CH₂Cl₂ / 24 h / Ambient temperature

8: 1.) n-BuLi / 1.) THF, -78 deg C, 60 min, 2.) THF, a) -78 deg C, 30 min, b) RT, 45 min

9: 89 percent / concd H₂SO₄ / 24 h / Heating

10: 95 percent / LiAlH₄ / diethyl ether / 4 h / Heating

11: 85 percent / Me₃SiI / CH₂Cl₂ / 24 h / Ambient temperature

12: 82 percent / dimethylsulfoxide / 2 h / 80 °C

13: 91 percent / KOH / ethane-1,2-diol / 6 h / Heating

14: 95 percent / diethyl ether / 12 h / 0 °C

15: 1.) Tl(OCOCF₃)3, 2.) aq. KI / 1.) TFA, RT, 5 d, 2.) TFA, 15 min

With potassium hydroxide; lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; thionyl chloride; trimethylsilyl iodide; sulfuric acid; hydrazine hydrate; potassium iodide; thallium(III) trifluoroacetate; In diethyl ether; dichloromethane; ethylene glycol; dimethyl sulfoxide; N,N-dimethyl-formamide; diethylene glycol;
DOI:10.1021/jm00369a027

Reference yield:

: 15949-84-5
11-bromoundecanoyl chloride

: 88336-93-0
methyl 15-(p-iodophenyl)-3(RS)-methylpentadecanoate

Guidance literature:: Multi-step reaction with 14 steps

1: AlCl₃ / dimethylformamide / 1 h / 90 °C

2: 85 percent / dimethylsulfoxide / 2 h / 80 °C

3: 95 percent / NH₂NH₂*H₂O, KOH / bis-(2-hydroxy-ethyl) ether / 4 h / Heating

4: 95 percent / diethyl ether / 12 h / 0 °C

5: 90 percent / LiAlH₄ / diethyl ether / 4 h / Heating

6: 88 percent / Me₃SiI / CH₂Cl₂ / 24 h / Ambient temperature

7: 1.) n-BuLi / 1.) THF, -78 deg C, 60 min, 2.) THF, a) -78 deg C, 30 min, b) RT, 45 min

8: 89 percent / concd H₂SO₄ / 24 h / Heating

9: 95 percent / LiAlH₄ / diethyl ether / 4 h / Heating

10: 85 percent / Me₃SiI / CH₂Cl₂ / 24 h / Ambient temperature

11: 82 percent / dimethylsulfoxide / 2 h / 80 °C

12: 91 percent / KOH / ethane-1,2-diol / 6 h / Heating

13: 95 percent / diethyl ether / 12 h / 0 °C

14: 1.) Tl(OCOCF₃)3, 2.) aq. KI / 1.) TFA, RT, 5 d, 2.) TFA, 15 min

With potassium hydroxide; lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; trimethylsilyl iodide; sulfuric acid; hydrazine hydrate; potassium iodide; thallium(III) trifluoroacetate; In diethyl ether; dichloromethane; ethylene glycol; dimethyl sulfoxide; N,N-dimethyl-formamide; diethylene glycol;
DOI:10.1021/jm00369a027

Reference yield:

: 14507-27-8
12-Phenyldodecanoic Acid

: 88336-93-0
methyl 15-(p-iodophenyl)-3(RS)-methylpentadecanoate

Guidance literature:: Multi-step reaction with 11 steps

1: 95 percent / diethyl ether / 12 h / 0 °C

2: 90 percent / LiAlH₄ / diethyl ether / 4 h / Heating

3: 88 percent / Me₃SiI / CH₂Cl₂ / 24 h / Ambient temperature

4: 1.) n-BuLi / 1.) THF, -78 deg C, 60 min, 2.) THF, a) -78 deg C, 30 min, b) RT, 45 min

5: 89 percent / concd H₂SO₄ / 24 h / Heating

6: 95 percent / LiAlH₄ / diethyl ether / 4 h / Heating

7: 85 percent / Me₃SiI / CH₂Cl₂ / 24 h / Ambient temperature

8: 82 percent / dimethylsulfoxide / 2 h / 80 °C

9: 91 percent / KOH / ethane-1,2-diol / 6 h / Heating

10: 95 percent / diethyl ether / 12 h / 0 °C

11: 1.) Tl(OCOCF₃)3, 2.) aq. KI / 1.) TFA, RT, 5 d, 2.) TFA, 15 min

With potassium hydroxide; lithium aluminium tetrahydride; n-butyllithium; trimethylsilyl iodide; sulfuric acid; potassium iodide; thallium(III) trifluoroacetate; In diethyl ether; dichloromethane; ethylene glycol; dimethyl sulfoxide;
DOI:10.1021/jm00369a027