5-(4-bromobenzoyl)-1,3-dimethyl-6-(2-morpholinoethenyl)-pyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:5-(4-bromobenzoyl)-1,3-dimethyl-6-(2-morpholinoethenyl)-pyrimidine-2,4(1H,3H)-dione
CAS No.:835896-29-2
Molecular Formula:C₁₉H₂₀BrN₃O₄
Molecular Weight:434.289
Hs Code.:

Synonyms:5-(4-bromobenzoyl)-1,3-dimethyl-6-(2-morpholinoethenyl)-pyrimidine-2,4(1H,3H)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-bromobenzoyl)-1,3-dimethyl-6-(2-morpholinoethenyl)-pyrimidine-2,4(1H,3H)-dione

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Technology Process of 5-(4-bromobenzoyl)-1,3-dimethyl-6-(2-morpholinoethenyl)-pyrimidine-2,4(1H,3H)-dione

There total 1 articles about 5-(4-bromobenzoyl)-1,3-dimethyl-6-(2-morpholinoethenyl)-pyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 110-91-8,99108-56-2
morpholine

: 833437-35-7
C₁₄H₁₃BrN₂O₃

: 122-51-0
orthoformic acid triethyl ester

: 835896-29-2
5-(4-bromobenzoyl)-1,3-dimethyl-6-(2-morpholinoethenyl)-pyrimidine-2,4(1H,3H)-dione

Guidance literature:: for 2h; Reflux;
DOI:10.1007/s11172-008-0232-3

Reference yield: 94.0%

: 835896-29-2
5-(4-bromobenzoyl)-1,3-dimethyl-6-(2-morpholinoethenyl)-pyrimidine-2,4(1H,3H)-dione

: 1112111-23-5
5-(4-bromophenyl)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrano[4,3-d]pyrimidin-6-ium perchlorate

Guidance literature:: With perchloric acid; In orthoformic acid triethyl ester; for 0.0833333h; Reflux;
DOI:10.1007/s11172-008-0232-3

Reference yield:

: 835896-29-2
5-(4-bromobenzoyl)-1,3-dimethyl-6-(2-morpholinoethenyl)-pyrimidine-2,4(1H,3H)-dione

: 1112111-49-5
6-amino-5-(4-bromophenyl)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrido[4,3-d]pyrimidin-6-ium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: perchloric acid / orthoformic acid triethyl ester / 0.08 h / Reflux

2: hydrazine hydrate; acetic acid / 0.08 h / Reflux

With perchloric acid; hydrazine hydrate; acetic acid; In orthoformic acid triethyl ester;
DOI:10.1007/s11172-008-0232-3