2-[[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]oxy]-2-methylpropanamide

Base Information

• Chemical Name: 2-[[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]oxy]-2-methylpropanamide
• CAS No.: 98626-62-1
• Molecular Formula: C₂₁H₂₅ClN₂O₂
• Molecular Weight: 372.895

Synonyms:2-[[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]oxy]-2-methylpropanamide

Chemical Property of 2-[[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]oxy]-2-methylpropanamide

Chemical Property:

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Technology Process of 2-[[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]oxy]-2-methylpropanamide

There total 2 articles about 2-[[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]oxy]-2-methylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-2-methylpropanamide (7462-74-0) + SCH 23390 (73445-63-3,84384-04-3,87075-17-0,95191-55-2) → 2-[[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]oxy]-2-methylpropanamide (98626-62-1)

Guidance literature:

SCH 23390; With sodium hydride; In 1,4-dioxane; at 20 ℃; for 1h;

2-bromo-2-methylpropanamide; In 1,4-dioxane; Heating;

DOI:10.1021/jm030614p

Reference yield:

→ 2-[[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]oxy]-2-methylpropanamide (98626-62-1)

Guidance literature:

Reference yield:

2-[[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]oxy]-2-methylpropanamide (98626-62-1) → N-[8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-yl]-2-hydroxy-2-methylpropanamide

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 50 ℃;

DOI:10.1021/jm030614p

upstream raw materials:

2-bromo-2-methylpropanamide

SCH 23390

Downstream raw materials:

8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-amine

6-bromo-8-chloro-2,3,4,5-tetrahydro-3-methyl-5(R)-phenyl-1H-3-benzazepin-7-amine

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