benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate

Base Information

Chemical Name:benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate
CAS No.:83102-08-3
Molecular Formula:C₂₁H₂₇NO₆
Molecular Weight:389.448
Hs Code.:

Synonyms:benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate

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Chemical Property of benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate

Chemical Property:

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Technology Process of benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate

There total 9 articles about benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 83102-07-2
benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-oxopiperidine-1-carboxylate

: 83102-08-3
benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate

Guidance literature:: With sodium hydride; In benzene; for 1h; Ambient temperature;
DOI:10.1248/cpb.31.1551

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 83102-08-3
benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) MCPBA; 3.) B₂H₆, NaBH₄ / 2.) CH₂Cl₂, rt, 15 h; 3.) THF, rt, 3 h

2: PCC

3: benzene

With sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; diborane; In benzene;
DOI:10.1248/cpb.30.1925

Reference yield:

: 83102-06-1
benzyl 5-(1,3-dioxolan-2-ylmethyl)-4-hydroxypiperidine-1-carboxylate

: 83102-08-3
benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: PCC

2: benzene

With pyridinium chlorochromate; In benzene;
DOI:10.1248/cpb.30.1925