[Mo(phenyl isocyanide)5(1,2-bis(diphenylphosphino)ethane)](hexafluorophosphate)2

Base Information

Chemical Name:[Mo(phenyl isocyanide)5(1,2-bis(diphenylphosphino)ethane)](hexafluorophosphate)2
CAS No.:79721-80-5
Molecular Formula:C₆₁H₄₉MoN₅P₂*2F₆P
Molecular Weight:1299.91
Hs Code.:

Synonyms:[Mo(phenyl isocyanide)5(1,2-bis(diphenylphosphino)ethane)](hexafluorophosphate)2

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Chemical Property of [Mo(phenyl isocyanide)5(1,2-bis(diphenylphosphino)ethane)](hexafluorophosphate)2

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Technology Process of [Mo(phenyl isocyanide)5(1,2-bis(diphenylphosphino)ethane)](hexafluorophosphate)2

There total 1 articles about [Mo(phenyl isocyanide)5(1,2-bis(diphenylphosphino)ethane)](hexafluorophosphate)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 78653-88-0
Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-)

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 79721-80-5
[Mo(phenyl isocyanide)5(1,2-bis(diphenylphosphino)ethane)](hexafluorophosphate)2

Guidance literature:: In ethanol; byproducts: C6H5CN; under N2, refluxed for 30 min; cooled to room temp., prod. filtered, washed with diethyl ether, dried in vac., elem.anal.;

Reference yield: 50.0%

: 79721-80-5
[Mo(phenyl isocyanide)5(1,2-bis(diphenylphosphino)ethane)](hexafluorophosphate)2

: [molybdenum (tetrakis(phenyl isocyanide))(1,2-bis(diphenylphosphino)ethane)]

Guidance literature:: With magnesium; In tetrahydrofuran; under N2, addn. of Mg metal, THF, 1,2-dibromoethane, stirring the mixt.for 15 min, then addn. of 1,2-dibromoethane, stirring at room temp. in the dark for 4 h; chromy. on alumina under oxygen-free conditions, (elution with benzene), solvent removed under N2, oil treated with ethanol, solid collected and dried in vac., identified by IR and 1H NMR;