(3R,4S)-3-(benzyloxycarbonylamino)-4-hydroxypyrrolidine-1-formic acid tert-butyl ester

Base Information

• Chemical Name: (3R,4S)-3-(benzyloxycarbonylamino)-4-hydroxypyrrolidine-1-formic acid tert-butyl ester
• CAS No.: 952443-90-2
• Molecular Formula: C₁₇H₂₄N₂O₅
• Molecular Weight: 336.388

Synonyms:(3R,4S)-3-(benzyloxycarbonylamino)-4-hydroxypyrrolidine-1-formic acid tert-butyl ester

Chemical Property of (3R,4S)-3-(benzyloxycarbonylamino)-4-hydroxypyrrolidine-1-formic acid tert-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (3R,4S)-3-(benzyloxycarbonylamino)-4-hydroxypyrrolidine-1-formic acid tert-butyl ester

There total 2 articles about (3R,4S)-3-(benzyloxycarbonylamino)-4-hydroxypyrrolidine-1-formic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butyl (3R,4S)-3-benzyloxycarbonylamino-4-(t-butyldimethylsilanoxy)pyrrolidine-1-carboxylate → (3R,4S)-3-(benzyloxycarbonylamino)-4-hydroxypyrrolidine-1-formic acid tert-butyl ester (952443-90-2)

Guidance literature:

t-butyl (3R,4S)-3-benzyloxycarbonylamino-4-(t-butyldimethylsilanoxy)pyrrolidine-1-carboxylate; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 3.5h;

With water;

Reference yield:

→ (3R,4S)-3-(benzyloxycarbonylamino)-4-hydroxypyrrolidine-1-formic acid tert-butyl ester (952443-90-2)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; water; at 0 - 25 ℃; for 1h;

Reference yield:

(3R,4S)-3-(benzyloxycarbonylamino)-4-hydroxypyrrolidine-1-formic acid tert-butyl ester (952443-90-2) → benzyl ((3R,4S)-4-hydroxypyrrolidin-3-yl)carbamate (1412256-94-0,1810070-09-7)

Guidance literature:

With hydrogenchloride; In methanol; at 26 ℃; for 16h;

Downstream raw materials:

t-butyl (3R,4S)-3-benzyloxycarbonylamino-4-methanesulfonyloxypyrrolidine-1-carboxylate

benzyl ((3R,4S)-4-hydroxypyrrolidin-3-yl)carbamate

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