(1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid

Base Information

Chemical Name:(1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid
CAS No.:1170695-88-1
Molecular Formula:C₂₆H₃₁NO₇
Molecular Weight:469.535
Hs Code.:

Synonyms:(1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid

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Chemical Property of (1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid

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Technology Process of (1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid

There total 1 articles about (1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1170695-89-2
C₂₆H₃₃NO₆

: 1170695-88-1
(1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid

Guidance literature:: With chromic acid; In water; acetone; Cooling with ice;
DOI:10.1016/j.tetasy.2009.03.009

Reference yield: 100.0%

: 1170695-88-1
(1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid

: 18107-18-1
diazomethyl-trimethyl-silane

: 1170695-93-8
(1S,3S,4S,5R,6S,7S)-methyl 4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylate

Guidance literature:: In methanol; hexane; toluene; for 1h;
DOI:10.1016/j.tetasy.2009.03.009

Reference yield:

: C₂₂H₂₅NO₅

: 1170695-88-1
(1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid

: 1170695-94-9
(1S,3S,4S,5R,6S,7S)-methyl 4,5-bis(benzyloxy)-7-((1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butoxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxamido)-2-oxabicyclo[4.1.0]heptane-3-carboxylate

Guidance literature:: (1S,3S,4S,5R,6S,7S)-4,5-bis(benzyloxy)-7-(tert-butyloxycarbonylamino)-2-oxabicyclo[4.1.0]heptane-3-carboxylic acid; With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; N,N-dimethyl-formamide; for 0.0833333h;

C₂₂H₂₅NO₅; In dichloromethane; N,N-dimethyl-formamide; for 16h;
DOI:10.1016/j.tetasy.2009.03.009