N²-<(R)-2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carbonyl>-(S)-phenylalanine cyclohexylamide

Base Information

• Chemical Name: N²-<(R)-2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carbonyl>-(S)-phenylalanine cyclohexylamide
• CAS No.: 168629-01-4
• Molecular Formula: C₃₄H₃₉N₃O₄
• Molecular Weight: 553.701

Synonyms:N²-<(R)-2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carbonyl>-(S)-phenylalanine cyclohexylamide

Chemical Property of N²-<(R)-2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carbonyl>-(S)-phenylalanine cyclohexylamide

Chemical Property:

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Technology Process of N²-<(R)-2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carbonyl>-(S)-phenylalanine cyclohexylamide

There total 1 articles about N²-<(R)-2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carbonyl>-(S)-phenylalanine cyclohexylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

L-phenylalanine cyclohexylamide (17186-53-7,92698-80-1) + C19H17NO3 (168628-99-7) → N2-<(R)-2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carbonyl>-(S)-phenylalanine cyclohexylamide (168629-01-4) + N2-[(S)-2-benzamido-8-methoxy-1,2,3,4-tetrahydro-naphthalene-2-carbonyl]-L-phenylalanine cyclohexylamide

Guidance literature:

With 1-methyl-pyrrolidin-2-one; at 90 ℃; for 36h;

DOI:10.1002/hlca.19950780613

Reference yield: 93.0%

N2-<(R)-2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carbonyl>-(S)-phenylalanine cyclohexylamide (168629-01-4) → (R)-methyl 2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carboxylate (144732-13-8)

Guidance literature:

With trifluorormethanesulfonic acid; In methanol; at 80 ℃; for 20h;

DOI:10.1002/hlca.19950780613

upstream raw materials:

L-phenylalanine cyclohexylamide

C₁₉H₁₇NO₃

Downstream raw materials:

(R)-methyl 2-benzamido-1,2,3,4-tetrahydro-8-methoxynaphthalene-2-carboxylate

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