Ni(acetylacetone^(1-))(N,N,N',N'-tetramethylethylenediamine)2B(C₆H₅)4

Base Information

• Chemical Name: Ni(acetylacetone^(1-))(N,N,N',N'-tetramethylethylenediamine)2B(C₆H₅)4
• CAS No.: 906750-67-2
• Molecular Formula: C₁₇H₃₉N₄NiO₂*C₂₄H₂₀B
• Molecular Weight: 709.446
• Mol file: 906750-67-2.mol

Synonyms:Ni(acetylacetone^(1-))(N,N,N',N'-tetramethylethylenediamine)2B(C₆H₅)4

Chemical Property of Ni(acetylacetone^(1-))(N,N,N',N'-tetramethylethylenediamine)2B(C₆H₅)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Ni(acetylacetone^(1-))(N,N,N',N'-tetramethylethylenediamine)2B(C₆H₅)4

There total 1 articles about Ni(acetylacetone^(1-))(N,N,N',N'-tetramethylethylenediamine)2B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

{Ni(acac)(tmen)}(BPh4) + N,N,N,N,-tetramethylethylenediamine (110-18-9) → Ni(acetylacetone(1-))(N,N,N',N'-tetramethylethylenediamine)2B(C6H5)4 (906750-67-2)

Guidance literature:

In ethanol; 1,2-dichloro-ethane; soln. of ligand in EtOH added to DCE soln. of Ni-complex, stirred for 30min; filtered, left overnight, recrystd. from DCE; elem. anal.;

DOI:10.1016/j.saa.2005.09.015

Reference yield:

Ni(acetylacetone(1-))(N,N,N',N'-tetramethylethylenediamine)2B(C6H5)4 (906750-67-2) → nickel (7440-02-0)

Guidance literature:

In neat (no solvent, solid phase); Ni-complex heated at 800°C; monitored by XRD;

DOI:10.1016/j.saa.2005.09.015

upstream raw materials:

N,N,N,N,-tetramethylethylenediamine

Downstream raw materials:

nickel