2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside

Base Information

Chemical Name:2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside
CAS No.:1379653-39-0
Molecular Formula:C₇₈H₇₄NO₃₁S*Na
Molecular Weight:1576.49
Hs Code.:

2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside

Synonyms:2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside

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Chemical Property of 2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside

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Technology Process of 2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside

There total 1 articles about 2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1379653-37-8
2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside

: 108-24-7
acetic anhydride

: 1379653-39-0
2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside

Guidance literature:: 2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside; With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 40 ℃; for 10h;

acetic anhydride; With pyridine; at 20 ℃;

In methanol; dichloromethane; water;
DOI:10.1016/j.carres.2012.03.039

Reference yield: 86.0%

: 1379653-39-0
2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside

: 2-benzyloxycarbonylaminoethyl O-(sodium β-D-glucopyranosyluronate)-(1->3)-(β-D-galactopyranosyl)-(1->3)-6-O-sodium sulfonato-β-D-galactopyranoside

Guidance literature:: 2-benzyloxycarbonylaminoethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->3)-4-O-acetyl-2-O-benzoyl-6-O-sodium sulfonato-β-D-galactopyranoside; With dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; water; at -10 - 20 ℃; for 8h;

With sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 16h;
DOI:10.1016/j.carres.2012.03.039