Technology Process of 3-methyl-6-phenyl-3-azabicyclo<4,2,1>nonane
There total 6 articles about 3-methyl-6-phenyl-3-azabicyclo<4,2,1>nonane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide; hydrazine hydrate;
In
various solvent(s);
at 165 - 175 ℃;
for 4h;
heating 185-195 for another 4 hrs.;
DOI:10.1002/jhet.5570220312
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / sodium amide / benzene / Heating; stirring at reflux temp. overnight
2: 91 percent / benzene / 2 h / Heating
3: 100 percent / hydrochloric acid (12 N) / 20 h / 120 - 130 °C
4: 33 percent / acetic acid / 4 h / 100 °C
5: 75 percent / hydrazine hydrate (95 percent), potassium hydroxide / various solvent(s) / 4 h / 165 - 175 °C / heating 185-195 for another 4 hrs.
With
hydrogenchloride; potassium hydroxide; hydrazine hydrate; sodium amide; acetic acid;
In
benzene;
DOI:10.1002/jhet.5570220312
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / hydrochloric acid (12 N) / 20 h / 120 - 130 °C
2: 33 percent / acetic acid / 4 h / 100 °C
3: 75 percent / hydrazine hydrate (95 percent), potassium hydroxide / various solvent(s) / 4 h / 165 - 175 °C / heating 185-195 for another 4 hrs.
With
hydrogenchloride; potassium hydroxide; hydrazine hydrate; acetic acid;
In
various solvent(s);
DOI:10.1002/jhet.5570220312
