C₄₇H₄₄N₆O₈

Base Information

Chemical Name:C₄₇H₄₄N₆O₈
CAS No.:1367204-50-9
Molecular Formula:C₄₇H₄₄N₆O₈
Molecular Weight:820.902
Hs Code.:

C<sub>47</sub>H<sub>44</sub>N<sub>6</sub>O<sub>8</sub>

Synonyms:C₄₇H₄₄N₆O₈

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Chemical Property of C₄₇H₄₄N₆O₈

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Technology Process of C₄₇H₄₄N₆O₈

There total 6 articles about C₄₇H₄₄N₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1367204-38-3
C₂₆H₂₆N₆O₆

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1367204-50-9
C₄₇H₄₄N₆O₈

Guidance literature:: With pyridine; silver nitrate; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/cbic.201100573

Reference yield:

: 211676-15-2
8-bromo-3′,5′-O-bis(tert-butyldimethylsilyl)-2′-deoxyadenosine

: 1367204-50-9
C₄₇H₄₄N₆O₈

Guidance literature:: Multi-step reaction with 5 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 95 °C

2: pyridine / 20 °C / Inert atmosphere

3: pyridine; dmap / 20 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 48 h / 20 °C

5: pyridine; silver nitrate / 3 h / 20 °C / Inert atmosphere

With pyridine; dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrabutyl ammonium fluoride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; silver nitrate; acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; 1: Buchwald-Hartwig cross-coupling;
DOI:10.1002/cbic.201100573

Reference yield:

: 1367204-28-1
C₃₈H₅₄N₆O₆Si₂

: 1367204-50-9
C₄₇H₄₄N₆O₈

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 48 h / 20 °C

2: pyridine; silver nitrate / 3 h / 20 °C / Inert atmosphere

With pyridine; tetrabutyl ammonium fluoride; silver nitrate; acetic acid; In tetrahydrofuran;
DOI:10.1002/cbic.201100573