Pentacyclo(18.2.2.2(9,12).0(4,15).0(6,17))hexacosa-4,6(17),9,11,15,20,22,23,25-nonane

Base Information

Chemical Name:Pentacyclo(18.2.2.2(9,12).0(4,15).0(6,17))hexacosa-4,6(17),9,11,15,20,22,23,25-nonane
CAS No.:35117-21-6
Molecular Formula:C₂₆H₂₆
Molecular Weight:338.492
Hs Code.:
DSSTox Substance ID:DTXSID40188619
Wikidata:Q83060433
Mol file:35117-21-6.mol

Synonyms:Pentacyclo(18.2.2.2(9,12).0(4,15).0(6,17))hexacosa-4,6(17),9,11,15,20,22,23,25-nonane;35117-21-6;Pentacyclo[18.2.2.2(9,12).0(4,15).0(6,17)]hexacosa-4,6(17),9,11,15,20,22,23,25-nonane;DTXSID40188619

Suppliers and Price of Pentacyclo(18.2.2.2(9,12).0(4,15).0(6,17))hexacosa-4,6(17),9,11,15,20,22,23,25-nonane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Pentacyclo(18.2.2.2(9,12).0(4,15).0(6,17))hexacosa-4,6(17),9,11,15,20,22,23,25-nonane

Chemical Property:

Vapor Pressure:1.46E-08mmHg at 25°C
Boiling Point:470.2°Cat760mmHg
Flash Point:236.5°C
Density:1.079g/cm³
XLogP3:6.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:338.203450829
Heavy Atom Count:26
Complexity:405

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=CC3=C(CCC4=CC=C1C=C4)C=C2CCC5=CC=CC(=C5)CC3

Technology Process of Pentacyclo(18.2.2.2(9,12).0(4,15).0(6,17))hexacosa-4,6(17),9,11,15,20,22,23,25-nonane

There total 9 articles about Pentacyclo(18.2.2.2(9,12).0(4,15).0(6,17))hexacosa-4,6(17),9,11,15,20,22,23,25-nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 121511-54-4
triple-layered tetrathia<3.3><3.3>paracyclophane

: 35117-21-6,36757-08-1,774128-72-2
[2.2][2.2]paracyclophane

Guidance literature:: With triethyl phosphite; In benzene; for 5h; Irradiation;
DOI:10.1246/bcsj.62.164

Reference yield: 80.0%

: 85555-53-9
C₂₆H₂₆Se₂

: 35117-21-6,36757-08-1,774128-72-2
[2.2][2.2]paracyclophane

Guidance literature:: With Hexamethylphosphorous triamide; In tetrahydrofuran; for 23h; Irradiation;
DOI:10.1016/S0040-4039(00)81990-5

Reference yield:

: 15442-91-8
1,2,4,5-tetrabromomethylbenzene

: 35117-21-6,36757-08-1,774128-72-2
[2.2][2.2]paracyclophane

Guidance literature:: Multi-step reaction with 4 steps

1: 2.21 g / aq. ethanol / 5 h / Heating

2: KOH / H₂O / 4 h / Heating

3: 12 percent / KOH / benzene; ethanol / 12 h / Heating

4: 93 percent / triethyl phosphite / benzene / 5 h / Irradiation

With potassium hydroxide; triethyl phosphite; In ethanol; water; benzene;
DOI:10.1246/bcsj.62.164