(4R,2E)-1-ethyl-8-methyl-4-(N,N₀-(dibenzyloxycarbonyl)hydrazinyl)oct-2-enedioate

Base Information

• Chemical Name: (4R,2E)-1-ethyl-8-methyl-4-(N,N₀-(dibenzyloxycarbonyl)hydrazinyl)oct-2-enedioate
• CAS No.: 1260143-46-1
• Molecular Formula: C₂₇H₃₂N₂O₈
• Molecular Weight: 512.56

Synonyms:(4R,2E)-1-ethyl-8-methyl-4-(N,N₀-(dibenzyloxycarbonyl)hydrazinyl)oct-2-enedioate

Chemical Property of (4R,2E)-1-ethyl-8-methyl-4-(N,N₀-(dibenzyloxycarbonyl)hydrazinyl)oct-2-enedioate

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Technology Process of (4R,2E)-1-ethyl-8-methyl-4-(N,N₀-(dibenzyloxycarbonyl)hydrazinyl)oct-2-enedioate

There total 1 articles about (4R,2E)-1-ethyl-8-methyl-4-(N,N₀-(dibenzyloxycarbonyl)hydrazinyl)oct-2-enedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

diethoxyphosphoryl-acetic acid ethyl ester (867-13-0) + methyl 6-oxohexanoate (6654-36-0) + dibenzyl azodicarboxylate (2449-05-0) → (4R,2E)-1-ethyl-8-methyl-4-(N,N0-(dibenzyloxycarbonyl)hydrazinyl)oct-2-enedioate (1260143-46-1)

Guidance literature:

methyl 6-oxohexanoate; dibenzyl azodicarboxylate; With L-proline; In acetonitrile; at 0 - 10 ℃; for 3h;

diethoxyphosphoryl-acetic acid ethyl ester; With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide; In acetonitrile; at 5 ℃; for 0.75h; enantioselective reaction;

DOI:10.1016/j.tetasy.2010.08.009

upstream raw materials:

diethoxyphosphoryl-acetic acid ethyl ester

methyl 6-oxohexanoate

dibenzyl azodicarboxylate

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