methyl [β-D-glucopyranosyl-(1->4)-β-(1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(β-D-glucopyranoside)]

Base Information

• Chemical Name: methyl [β-D-glucopyranosyl-(1->4)-β-(1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(β-D-glucopyranoside)]
• CAS No.: 1315206-08-6
• Molecular Formula: C₂₀H₃₄O₁₄S
• Molecular Weight: 530.548

Synonyms:methyl [β-D-glucopyranosyl-(1->4)-β-(1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(β-D-glucopyranoside)]

Chemical Property of methyl [β-D-glucopyranosyl-(1->4)-β-(1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(β-D-glucopyranoside)]

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Technology Process of methyl [β-D-glucopyranosyl-(1->4)-β-(1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(β-D-glucopyranoside)]

There total 1 articles about methyl [β-D-glucopyranosyl-(1->4)-β-(1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(β-D-glucopyranoside)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

methyl [[2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-β-[2,3,6-tris-O-(4-methoxyphenylmethyl)-1-thio-Δ(5,5a)carbaglucopyranosyl]-(1->4)-β-[2,3,6-O-tris-(4-methoxyphenylmethyl)-β-D-glucopyranoside]] (1315206-22-4) → methyl [β-D-glucopyranosyl-(1->4)-β-(1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(β-D-glucopyranoside)] (1315206-08-6)

Guidance literature:

With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 13h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.04.048

Reference yield: 87.0%

methyl [β-D-glucopyranosyl-(1->4)-β-(1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(β-D-glucopyranoside)] (1315206-08-6) + acetic anhydride (108-24-7) → methyl [2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-β-(2,3,6-O-triacetyl-1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(2,3,6-tri-O-acetyl-β-D-glucopyranoside)] (1315205-99-2)

Guidance literature:

With pyridine; dmap; at 60 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.04.048

upstream raw materials:

methyl [[2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-β-[2,3,6-tris-O-(4-methoxyphenylmethyl)-1-thio-Δ(5,5a)carbaglucopyranosyl]-(1->4)-β-[2,3,6-O-tris-(4-methoxyphenylmethyl)-β-D-glucopyranoside]]

Downstream raw materials:

methyl [2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-β-(2,3,6-O-triacetyl-1-thio-Δ(5,5a)carbaglucopyranosyl)-(1->4)-β-(2,3,6-tri-O-acetyl-β-D-glucopyranoside)]

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