ethyl {3-[6-oxo-3-(4-cyanophenyl)-6H-pyridazin-1-ylmethyl]phenyl}carbamate

Base Information

• Chemical Name: ethyl {3-[6-oxo-3-(4-cyanophenyl)-6H-pyridazin-1-ylmethyl]phenyl}carbamate
• CAS No.: 1087379-64-3
• Molecular Formula: C₂₁H₁₈N₄O₃
• Molecular Weight: 374.399

Synonyms:ethyl {3-[6-oxo-3-(4-cyanophenyl)-6H-pyridazin-1-ylmethyl]phenyl}carbamate

Chemical Property of ethyl {3-[6-oxo-3-(4-cyanophenyl)-6H-pyridazin-1-ylmethyl]phenyl}carbamate

Chemical Property:

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Technology Process of ethyl {3-[6-oxo-3-(4-cyanophenyl)-6H-pyridazin-1-ylmethyl]phenyl}carbamate

There total 1 articles about ethyl {3-[6-oxo-3-(4-cyanophenyl)-6H-pyridazin-1-ylmethyl]phenyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(1,6-dihydro-6-oxo-3-pyridazinyl)benzonitrile (52240-10-5) + (3-hydroxymethyl-phenyl)-carbamic acid ethylester (81863-43-6) → ethyl {3-[6-oxo-3-(4-cyanophenyl)-6H-pyridazin-1-ylmethyl]phenyl}carbamate (1087379-64-3)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

ethyl {3-[6-oxo-3-(4-cyanophenyl)-6H-pyridazin-1-ylmethyl]phenyl}carbamate (1087379-64-3) → ethyl {3-[3-(4-aminomethylphenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate (1087377-48-7)

Guidance literature:

With ammonia; hydrogen; In methanol; at 20 ℃; for 16h; under 3750.38 Torr;

Reference yield:

ethyl {3-[6-oxo-3-(4-cyanophenyl)-6H-pyridazin-1-ylmethyl]phenyl}carbamate (1087379-64-3) → ethyl (3-{3-[4-(N-hydroxycarbamimidoyl)phenyl]-6-oxo-6H-pyridazin-1-yl-methyl}phenyl)carbamate (1087379-83-6)

Guidance literature:

With hydroxylamine hydrochloride; triethylamine; In ethanol; at 20 ℃; for 48h;

upstream raw materials:

4-(1,6-dihydro-6-oxo-3-pyridazinyl)benzonitrile

(3-hydroxymethyl-phenyl)-carbamic acid ethylester

Downstream raw materials:

ethyl (3-{3-[4-(N-hydroxycarbamimidoyl)phenyl]-6-oxo-6H-pyridazin-1-yl-methyl}phenyl)carbamate

ethyl (3-{6-oxo-3-[4-(1H-tetrazol-5-yl)phenyl]-6H-pyridazin-1-ylmethyl}phenyl)carbamate

ethyl {3-[3-(4-aminomethylphenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate

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