Hexadecanoic acid 4-amino-3-[1,3]dioxolan-2-yl-phenyl ester

Base Information

• Chemical Name: Hexadecanoic acid 4-amino-3-[1,3]dioxolan-2-yl-phenyl ester
• CAS No.: 205034-15-7
• Molecular Formula: C₂₅H₄₁NO₄
• Molecular Weight: 419.605
• Mol file: 205034-15-7.mol

Synonyms:Hexadecanoic acid 4-amino-3-[1,3]dioxolan-2-yl-phenyl ester

Chemical Property of Hexadecanoic acid 4-amino-3-[1,3]dioxolan-2-yl-phenyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Hexadecanoic acid 4-amino-3-[1,3]dioxolan-2-yl-phenyl ester

There total 4 articles about Hexadecanoic acid 4-amino-3-[1,3]dioxolan-2-yl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

Hexadecanoic acid 3-[1,3]dioxolan-2-yl-4-nitro-phenyl ester → Hexadecanoic acid 4-amino-3-[1,3]dioxolan-2-yl-phenyl ester (205034-15-7)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethyl acetate;

DOI:10.1016/S0960-894X(98)00039-0

Reference yield:

palmitic anhydride (623-65-4) → Hexadecanoic acid 4-amino-3-[1,3]dioxolan-2-yl-phenyl ester (205034-15-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / pyridine

2: p-TsOH / toluene / Heating

3: 63 percent / H₂ / PtO₂ / ethyl acetate

With pyridine; hydrogen; toluene-4-sulfonic acid; platinum(IV) oxide; In ethyl acetate; toluene;

DOI:10.1016/S0960-894X(98)00039-0

Reference yield:

2-nitro-5-hydroxybenzaldehyde (42454-06-8) → Hexadecanoic acid 4-amino-3-[1,3]dioxolan-2-yl-phenyl ester (205034-15-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / pyridine

2: p-TsOH / toluene / Heating

3: 63 percent / H₂ / PtO₂ / ethyl acetate

With pyridine; hydrogen; toluene-4-sulfonic acid; platinum(IV) oxide; In ethyl acetate; toluene;

DOI:10.1016/S0960-894X(98)00039-0

upstream raw materials:

palmitic anhydride

2-nitro-5-hydroxybenzaldehyde

Hexadecanoic acid 3-formyl-4-nitro-phenyl ester