C₃₇H₄₂O₉

Base Information

Chemical Name:C₃₇H₄₂O₉
CAS No.:162088-48-4
Molecular Formula:C₃₇H₄₂O₉
Molecular Weight:630.735
Hs Code.:

C<sub>37</sub>H<sub>42</sub>O<sub>9</sub>

Synonyms:C₃₇H₄₂O₉

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Chemical Property of C₃₇H₄₂O₉

Chemical Property:

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Technology Process of C₃₇H₄₂O₉

There total 9 articles about C₃₇H₄₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 162088-47-3
C₄₃H₅₆O₉Si

: 162088-48-4
C₃₇H₄₂O₉

Guidance literature:: With pyridine hydrogenfluoride; In tetrahydrofuran; at 25 ℃; for 1h; Yield given;
DOI:10.1021/ja00107a009

Reference yield:

: 162088-38-2
C₃₀H₃₆O₉

: 162088-48-4
C₃₇H₄₂O₉

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu₄NBH₄

2: 76 percent / KH, n-Bu₄NI / diethyl ether; hexamethylphosphoric acid triamide / 4 h / 25 °C

3: 98 percent / DBU / methanol; CH₂Cl₂ / 3 h / 25 °C

4: DMAP / dimethylformamide / 1 h / 25 °C

5: DMAP / CH₂Cl₂ / 0.5 h / 25 °C

6: HF*pyridine / tetrahydrofuran / 1 h / 25 °C

With dmap; tetra-(n-butyl)ammonium iodide; potassium hydride; tetrabutylammonium borohydride; Dess-Martin periodane; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00107a009

Reference yield:

: 162088-37-1
C₃₃H₄₂O₉

: 162088-48-4
C₃₇H₄₂O₉

Guidance literature:: Multi-step reaction with 8 steps

1: 93 percent / tetrapropylammonium perruthenate, 4-methylmorpholine N-oxide / acetonitrile / 2 h / 25 °C

2: p-toluenesulfonic acid / methanol / 48 h / 25 °C

3: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu₄NBH₄

4: 76 percent / KH, n-Bu₄NI / diethyl ether; hexamethylphosphoric acid triamide / 4 h / 25 °C

5: 98 percent / DBU / methanol; CH₂Cl₂ / 3 h / 25 °C

6: DMAP / dimethylformamide / 1 h / 25 °C

7: DMAP / CH₂Cl₂ / 0.5 h / 25 °C

8: HF*pyridine / tetrahydrofuran / 1 h / 25 °C

With dmap; tetrapropylammonium perruthennate; tetra-(n-butyl)ammonium iodide; potassium hydride; tetrabutylammonium borohydride; Dess-Martin periodane; toluene-4-sulfonic acid; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00107a009