Technology Process of C29H48O6SSi
There total 4 articles about C29H48O6SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tungstate; phenylphosphonate; dihydrogen peroxide;
In
toluene;
at 25 ℃;
for 2.5h;
DOI:10.1021/jo200934w
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine; carbon tetrabromide; triphenylphosphine / dichloromethane / 0.5 h / 25 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C
2.2: 3.5 h / 0 - 25 °C
3.1: sodium tungstate; phenylphosphonate; dihydrogen peroxide / toluene / 2.5 h / 25 °C
With
pyridine; sodium tungstate; carbon tetrabromide; phenylphosphonate; dihydrogen peroxide; sodium hydride; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; toluene; mineral oil;
1.1: Appel reaction;
DOI:10.1021/jo200934w
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C
1.2: 3.5 h / 0 - 25 °C
2.1: sodium tungstate; phenylphosphonate; dihydrogen peroxide / toluene / 2.5 h / 25 °C
With
sodium tungstate; phenylphosphonate; dihydrogen peroxide; sodium hydride;
In
tetrahydrofuran; toluene; mineral oil;
DOI:10.1021/jo200934w