(±)-6-(4-chlorophenyl)-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-2H-indazol-3-ol

Base Information

Chemical Name:(±)-6-(4-chlorophenyl)-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-2H-indazol-3-ol
CAS No.:1464082-60-7
Molecular Formula:C₂₂H₂₁ClN₂O₄
Molecular Weight:412.873
Hs Code.:

Synonyms:(±)-6-(4-chlorophenyl)-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-2H-indazol-3-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (±)-6-(4-chlorophenyl)-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-2H-indazol-3-ol

Chemical Property:

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Technology Process of (±)-6-(4-chlorophenyl)-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-2H-indazol-3-ol

There total 3 articles about (±)-6-(4-chlorophenyl)-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-2H-indazol-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1464082-55-0
(±)-ethyl 4-(4-chlorophenyl)-2-oxo-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate

: 1464082-60-7
(±)-6-(4-chlorophenyl)-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-2H-indazol-3-ol

Guidance literature:: With hydrazine hydrate; acetic acid; In ethanol; for 6h; Reflux;
DOI:10.2174/1573406411309050012

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1464082-60-7
(±)-6-(4-chlorophenyl)-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-2H-indazol-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / ethanol / 12 h / 20 °C

2.1: sodium ethanolate / 1 h / 20 °C

2.2: 5 h / Reflux

3.1: hydrazine hydrate; acetic acid / ethanol / 6 h / Reflux

With sodium ethanolate; hydrazine hydrate; acetic acid; sodium hydroxide; In ethanol;
DOI:10.2174/1573406411309050012

Reference yield:

: 57077-27-7
1-(4-chlorophenyl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

: 1464082-60-7
(±)-6-(4-chlorophenyl)-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-2H-indazol-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium ethanolate / 1 h / 20 °C

1.2: 5 h / Reflux

2.1: hydrazine hydrate; acetic acid / ethanol / 6 h / Reflux

With sodium ethanolate; hydrazine hydrate; acetic acid; In ethanol;
DOI:10.2174/1573406411309050012