(3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid

Base Information

• Chemical Name: (3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid
• CAS No.: 93287-37-7
• Molecular Formula: C₁₆H₂₃NO₅
• Molecular Weight: 309.362

Synonyms:(3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid

Chemical Property of (3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid

Chemical Property:

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Technology Process of (3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid

There total 11 articles about (3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

((1S,2S)-2,4-Dihydroxy-1-isobutyl-butyl)-carbamic acid benzyl ester (111854-91-2) → (3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid (93287-37-7)

Guidance literature:

With oxygen; sodium hydrogencarbonate; platinum; In water; Ambient temperature;

DOI:10.1039/C39870000311

Reference yield: 93.0%

statine (49642-07-1) + 2-benzyloxycarbonylsulfanyl-4,6-dimethyl-pyrimidine (42116-21-2) → (3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid (93287-37-7)

Guidance literature:

With triethylamine; In 1,4-dioxane; water; at 30 ℃;

DOI:10.1246/bcsj.63.2224

Reference yield: 48.0%

(1S,2S)-(2-hydroxy-1-isobutyl-pent-4-enyl)-carbamic acid benzyl ester (113283-66-2) → (3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid (93287-37-7)

Guidance literature:

With potassium permanganate; sulfuric acid; In acetone; at 0 ℃; for 0.0833333h;

DOI:10.1021/jo010383z

upstream raw materials:

Z-(4S,5S)-4-hydroxy-pyrrolidin-2-one

statine

2-benzyloxycarbonylsulfanyl-4,6-dimethyl-pyrimidine

((1S,2S)-2,4-Dihydroxy-1-isobutyl-butyl)-carbamic acid benzyl ester

Downstream raw materials:

(3S,4S)-4-Benzyloxycarbonylamino-3-hydroxy-6-methyl-heptanoic acid methyl ester

2-amino>-3-methylbutyl>phosphinyl>acetic acid methyl ester

statine

(4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine

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