3-<3-(benzyloxy)phenyl>-N-propylpiperidine

Base Information

Chemical Name:3-<3-(benzyloxy)phenyl>-N-propylpiperidine
CAS No.:110174-88-4
Molecular Formula:C₂₁H₂₇NO
Molecular Weight:309.451
Hs Code.:

Synonyms:3-<3-(benzyloxy)phenyl>-N-propylpiperidine

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Chemical Property of 3-<3-(benzyloxy)phenyl>-N-propylpiperidine

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Technology Process of 3-<3-(benzyloxy)phenyl>-N-propylpiperidine

There total 9 articles about 3-<3-(benzyloxy)phenyl>-N-propylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 79987-79-4
2-(3-benzyloxyphenyl)-N-propylglutarimide

: 110174-88-4
3-<3-(benzyloxy)phenyl>-N-propylpiperidine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 1.5h; Heating;
DOI:10.1002/recl.19811000909

Reference yield:

: 100-44-7
benzyl chloride

: 79412-27-4
(+/-)-3-PPP hydrobromide

: 110174-88-4
3-<3-(benzyloxy)phenyl>-N-propylpiperidine

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; for 1h; Heating;
DOI:10.1021/jm00394a014

Reference yield:

: 19924-43-7
3-methoxyphenylacetonitrile

: 110174-88-4
3-<3-(benzyloxy)phenyl>-N-propylpiperidine

Guidance literature:: Multi-step reaction with 8 steps

1: lithium diisopropylamide / tetrahydrofuran

2: 25percent sulfuric acid, 8N chromic acid / acetone

3: KOH / ethanol; H₂O / 6 h / Heating

4: 74 percent / acetic anhydride / 3 h / Heating

5: 2.) acetic anhydride / 1.) benzene, 1 h, reflux; 2.) 5 h, reflux

6: 93 percent / boron tribromide / CH₂Cl₂ / 2 h / Ambient temperature

7: 82 percent / potassium carbonate / dimethylformamide / 5 h

8: 91 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; sulfuric acid; acetic anhydride; boron tribromide; chromic acid; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/recl.19811000909