Technology Process of C33H39NO5
There total 5 articles about C33H39NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
4-methylmorpholine N-oxide;
tetrapropylammonium perruthennate;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene / Reflux
2.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2068.65 Torr / Inert atmosphere
2.2: 2 h / 20 °C / Cooling with ice
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Inert atmosphere; Cooling with ice
3.2: 20 °C / Cooling with ice
4.1: 4-methylmorpholine N-oxide / tetrapropylammonium perruthennate / dichloromethane / 2 h / 20 °C / Inert atmosphere; Cooling with ice
With
hydrogen; sodium hydride; 4-methylmorpholine N-oxide;
tetrapropylammonium perruthennate; palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 90 °C
2.1: toluene / Reflux
3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2068.65 Torr / Inert atmosphere
3.2: 2 h / 20 °C / Cooling with ice
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Inert atmosphere; Cooling with ice
4.2: 20 °C / Cooling with ice
5.1: 4-methylmorpholine N-oxide / tetrapropylammonium perruthennate / dichloromethane / 2 h / 20 °C / Inert atmosphere; Cooling with ice
With
hydrogen; sodium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide;
tetrapropylammonium perruthennate; palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;