diethyl 2-(((2R,3R,4R,5R)-4,5-bis(benzyloxy)-3-(methylsulfonyloxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(tert-butoxycarbonylamino)malonate

Base Information

Chemical Name:diethyl 2-(((2R,3R,4R,5R)-4,5-bis(benzyloxy)-3-(methylsulfonyloxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(tert-butoxycarbonylamino)malonate
CAS No.:1041478-16-3
Molecular Formula:C₃₃H₄₅NO₁₂S
Molecular Weight:679.786
Hs Code.:

Synonyms:diethyl 2-(((2R,3R,4R,5R)-4,5-bis(benzyloxy)-3-(methylsulfonyloxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(tert-butoxycarbonylamino)malonate

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Chemical Property of diethyl 2-(((2R,3R,4R,5R)-4,5-bis(benzyloxy)-3-(methylsulfonyloxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(tert-butoxycarbonylamino)malonate

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Technology Process of diethyl 2-(((2R,3R,4R,5R)-4,5-bis(benzyloxy)-3-(methylsulfonyloxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(tert-butoxycarbonylamino)malonate

There total 1 articles about diethyl 2-(((2R,3R,4R,5R)-4,5-bis(benzyloxy)-3-(methylsulfonyloxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(tert-butoxycarbonylamino)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1041478-14-1
C₂₁H₂₅BrO₆S

: 102831-44-7
diethyl tert-butoxycarbonylaminomalonate

: 1041478-16-3
diethyl 2-(((2R,3R,4R,5R)-4,5-bis(benzyloxy)-3-(methylsulfonyloxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(tert-butoxycarbonylamino)malonate

Guidance literature:: diethyl tert-butoxycarbonylaminomalonate; With sodium hydride; In toluene; at 0 ℃; for 0.75h;

C₂₁H₂₅BrO₆S; With tetra-(n-butyl)ammonium iodide; In toluene; for 14h; Further stages.; Heating;
DOI:10.1016/j.carres.2008.03.017