5(S)-<(tert-butoxycarbonyl)amino>-2(R)-methyl-6-<4-(phenylmethoxy)phenyl>-trans-3-hexenoic acid

Base Information

Chemical Name:5(S)-<(tert-butoxycarbonyl)amino>-2(R)-methyl-6-<4-(phenylmethoxy)phenyl>-trans-3-hexenoic acid
CAS No.:108385-60-0
Molecular Formula:C₂₅H₃₁NO₅
Molecular Weight:425.525
Hs Code.:

Synonyms:5(S)-<(tert-butoxycarbonyl)amino>-2(R)-methyl-6-<4-(phenylmethoxy)phenyl>-trans-3-hexenoic acid

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Chemical Property of 5(S)-<(tert-butoxycarbonyl)amino>-2(R)-methyl-6-<4-(phenylmethoxy)phenyl>-trans-3-hexenoic acid

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Technology Process of 5(S)-<(tert-butoxycarbonyl)amino>-2(R)-methyl-6-<4-(phenylmethoxy)phenyl>-trans-3-hexenoic acid

There total 17 articles about 5(S)-<(tert-butoxycarbonyl)amino>-2(R)-methyl-6-<4-(phenylmethoxy)phenyl>-trans-3-hexenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 109687-73-2
5(S)-<(tert-butoxycarbonyl)amino>-2(R)-methyl-6-<4-(phenylmethoxy)phenyl>-1-<(2-tetrahydropyranyl)oxy>-trans-3-hexene

: 108385-60-0
5(S)-<(tert-butoxycarbonyl)amino>-2(R)-methyl-6-<4-(phenylmethoxy)phenyl>-trans-3-hexenoic acid

Guidance literature:: With jones reagent; In acetone; at 0 ℃; for 3h;
DOI:10.1021/jo00226a007

Reference yield:

: [(E)-(S)-1-(4-Benzyloxy-benzyl)-5-hydroxy-4-methyl-pent-2-enyl]-carbamic acid tert-butyl ester

: 108385-60-0
(E)-(S)-6-(4-Benzyloxy-phenyl)-5-tert-butoxycarbonylamino-2-methyl-hex-3-enoic acid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In water; acetone; at 0 ℃; for 0.5h; Yield given;
DOI:10.1016/S0040-4039(00)84457-3

Reference yield:

: [(E)-(1S,4R)-1-(4-Benzyloxy-benzyl)-5-hydroxy-4-methyl-pent-2-enyl]-carbamic acid tert-butyl ester

: 108385-60-0
5(S)-<(tert-butoxycarbonyl)amino>-2(R)-methyl-6-<4-(phenylmethoxy)phenyl>-trans-3-hexenoic acid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In water; acetone; at 0 ℃; for 0.5h; Yield given;
DOI:10.1016/S0040-4039(00)84457-3