C₂HF₃O₂*C₁₀H₁₃N

Base Information

Chemical Name:C₂HF₃O₂*C₁₀H₁₃N
CAS No.:1373224-36-2
Molecular Formula:C₂HF₃O₂*C₁₀H₁₃N
Molecular Weight:261.244
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>10</sub>H<sub>13</sub>N

Synonyms:C₂HF₃O₂*C₁₀H₁₃N

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Chemical Property of C₂HF₃O₂*C₁₀H₁₃N

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Technology Process of C₂HF₃O₂*C₁₀H₁₃N

There total 1 articles about C₂HF₃O₂*C₁₀H₁₃N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 103127-52-2,107202-43-7
((S)-1-benzylallyl)carbamic acid tert-butyl ester

: 76-05-1
trifluoroacetic acid

: 1373224-36-2
C₂HF₃O₂*C₁₀H₁₃N

Guidance literature:: In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.02.007

Reference yield:

: 1373224-36-2
C₂HF₃O₂*C₁₀H₁₃N

: 80352-66-5
4-mesyloxy-2-methylbutene

: C₁₅H₂₁N

Guidance literature:: C₂HF₃O₂*C₁₀H₁₃N; With sodium hydrogencarbonate; In dichloromethane; water;

With potassium carbonate; In acetonitrile; at 20 ℃; for 1h;

4-mesyloxy-2-methylbutene; In acetonitrile; at 90 ℃; for 24h;
DOI:10.1016/j.tetasy.2012.02.007

Reference yield:

: 1373224-36-2
C₂HF₃O₂*C₁₀H₁₃N

: 1373224-41-9
C₂₅H₂₆NP

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate / dichloromethane; water

1.2: 1 h / 20 °C

1.3: 24 h / 90 °C

2.1: tetrahydrofuran / 21 h / 0 - 20 °C / Inert atmosphere

3.1: Grubbs catalyst first generation / benzene / 5 h / 60 °C / Inert atmosphere

4.1: dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: sodium hydroxide / diethyl ether; water

5.2: 24 h / 20 °C / Inert atmosphere

With Grubbs catalyst first generation; sodium hydrogencarbonate; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene;
DOI:10.1016/j.tetasy.2012.02.007