N-(4-Dimethylamino-phenyl)-formimidic acid 1,1-dimethyl-octadecyl ester

Base Information

• Chemical Name: N-(4-Dimethylamino-phenyl)-formimidic acid 1,1-dimethyl-octadecyl ester
• CAS No.: 82884-54-6
• Molecular Formula: C₂₉H₅₂N₂O
• Molecular Weight: 444.745
• Mol file: 82884-54-6.mol

Synonyms:N-(4-Dimethylamino-phenyl)-formimidic acid 1,1-dimethyl-octadecyl ester

Chemical Property of N-(4-Dimethylamino-phenyl)-formimidic acid 1,1-dimethyl-octadecyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-(4-Dimethylamino-phenyl)-formimidic acid 1,1-dimethyl-octadecyl ester

There total 2 articles about N-(4-Dimethylamino-phenyl)-formimidic acid 1,1-dimethyl-octadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-methylnonadecan-2-ol (76695-48-2) + 4-(dimethylamino)phenyl isocyanide (7050-85-3) → N-(4-Dimethylamino-phenyl)-formimidic acid 1,1-dimethyl-octadecyl ester (82884-54-6)

Guidance literature:

With copper(II) oxide; at 85 ℃;

DOI:10.1016/S0040-4039(00)87249-4

Reference yield:

Methyl stearate (112-61-8) → N-(4-Dimethylamino-phenyl)-formimidic acid 1,1-dimethyl-octadecyl ester (82884-54-6)

Guidance literature:

Multi-step reaction with 2 steps

2: 90 percent / CuO / 85 °C

With copper(II) oxide;

DOI:10.1016/S0040-4039(00)87249-4

Reference yield:

N-(4-Dimethylamino-phenyl)-formimidic acid 1,1-dimethyl-octadecyl ester (82884-54-6) → isoeicosane (1560-86-7,20574-75-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / H₂S, H₂SO₄ / pyridine / -10 - 0 °C

2: 83 percent / tributyltin hydride / benzene / Heating

With sulfuric acid; hydrogen sulfide; tri-n-butyl-tin hydride; In pyridine; benzene;

DOI:10.1016/S0040-4039(00)87249-4

upstream raw materials:

2-methylnonadecan-2-ol

4-(dimethylamino)phenyl isocyanide

Methyl stearate

Downstream raw materials:

isoeicosane