3-(benzyloxycarbonyloxy)-7-(bis(benzyloxy)phosphoryloxy)ursodeoxycholic acid benzyl ester

Base Information

Chemical Name:3-(benzyloxycarbonyloxy)-7-(bis(benzyloxy)phosphoryloxy)ursodeoxycholic acid benzyl ester
CAS No.:1486547-55-0
Molecular Formula:C₅₃H₆₅O₉P
Molecular Weight:877.067
Hs Code.:

Synonyms:3-(benzyloxycarbonyloxy)-7-(bis(benzyloxy)phosphoryloxy)ursodeoxycholic acid benzyl ester

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Chemical Property of 3-(benzyloxycarbonyloxy)-7-(bis(benzyloxy)phosphoryloxy)ursodeoxycholic acid benzyl ester

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Technology Process of 3-(benzyloxycarbonyloxy)-7-(bis(benzyloxy)phosphoryloxy)ursodeoxycholic acid benzyl ester

There total 6 articles about 3-(benzyloxycarbonyloxy)-7-(bis(benzyloxy)phosphoryloxy)ursodeoxycholic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1486547-53-8
3-(benzyloxycarbonyloxy)ursodeoxycholic acid benzyl ester

: 67746-43-4
dibenzyl N,N-diethylphosphoramidite

: 1486547-55-0
3-(benzyloxycarbonyloxy)-7-(bis(benzyloxy)phosphoryloxy)ursodeoxycholic acid benzyl ester

Guidance literature:: 3-(benzyloxycarbonyloxy)ursodeoxycholic acid benzyl ester; dibenzyl N,N-diethylphosphoramidite; With 1,2,4-Triazole; sodium hydrogencarbonate; In dichloromethane; at 40 ℃;

With dihydrogen peroxide; In tetrahydrofuran; water; at 0 ℃; for 0.0833333h;

Reference yield:

: C₅₃H₆₅O₈P

: 1486547-55-0
3-(benzyloxycarbonyloxy)-7-(bis(benzyloxy)phosphoryloxy)ursodeoxycholic acid benzyl ester

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; water; 1,2-dichloro-ethane; at 0 ℃; for 0.0833333h;
DOI:10.1002/cmdc.201300059

Reference yield:

: 128-13-2
ursodeoxycholic acid

: 1486547-55-0
3-(benzyloxycarbonyloxy)-7-(bis(benzyloxy)phosphoryloxy)ursodeoxycholic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 3 h / 80 °C

2: pyridine / dichloromethane / 1.5 h

3: 1,2,4-Triazole; sodium hydrogencarbonate / dichloromethane / 40 °C

4: dihydrogen peroxide / 1,2-dichloro-ethane; water; tetrahydrofuran / 0.08 h / 0 °C

With pyridine; 1,2,4-Triazole; dihydrogen peroxide; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1002/cmdc.201300059