potassium (2-ethoxyethyl)trifluoroborate

Base Information

• Chemical Name: potassium (2-ethoxyethyl)trifluoroborate
• CAS No.: 1408168-71-7
• Molecular Formula: C₄H₉BF₃O*K
• Molecular Weight: 180.019

Synonyms:potassium (2-ethoxyethyl)trifluoroborate

Chemical Property of potassium (2-ethoxyethyl)trifluoroborate

Chemical Property:

Purity/Quality:

99%,98%, ^*data from raw suppliers

Potassium(2-Ethoxyethyl)trifluoroborate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of potassium (2-ethoxyethyl)trifluoroborate

There total 1 articles about potassium (2-ethoxyethyl)trifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

potassium hydrogen difluoride + 2-(2-ethoxyethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1361022-71-0) → potassium (2-ethoxyethyl)trifluoroborate (1408168-71-7)

Guidance literature:

In tetrahydrofuran; water; at 20 ℃; for 2h;

DOI:10.1021/jo3021665

Reference yield: 88.0%

1-bromo-4-methoxy-benzene (104-92-7) + potassium (2-ethoxyethyl)trifluoroborate (1408168-71-7) → 1-(2-ethoxyethyl)-4-methoxybenzene (174460-92-5)

Guidance literature:

With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); caesium carbonate; In water; toluene; at 85 ℃; for 24h; Temperature; Inert atmosphere;

DOI:10.1021/jo3021665

upstream raw materials:

2-(2-ethoxyethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Downstream raw materials:

1-(2-ethoxyethyl)-4-methoxybenzene

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