1-(2-[allyl(toluene-4-sulfonyl)amino]phenyl)but-3-enylmethyl carbamic acid benzyl ester

Base Information

Chemical Name:1-(2-[allyl(toluene-4-sulfonyl)amino]phenyl)but-3-enylmethyl carbamic acid benzyl ester
CAS No.:1187201-03-1
Molecular Formula:C₂₉H₃₂N₂O₄S
Molecular Weight:504.65
Hs Code.:

Synonyms:1-(2-[allyl(toluene-4-sulfonyl)amino]phenyl)but-3-enylmethyl carbamic acid benzyl ester

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Chemical Property of 1-(2-[allyl(toluene-4-sulfonyl)amino]phenyl)but-3-enylmethyl carbamic acid benzyl ester

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Technology Process of 1-(2-[allyl(toluene-4-sulfonyl)amino]phenyl)but-3-enylmethyl carbamic acid benzyl ester

There total 1 articles about 1-(2-[allyl(toluene-4-sulfonyl)amino]phenyl)but-3-enylmethyl carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187201-02-0
C₁₈H₂₀N₂O₂S

: 18925-10-5
allylzinc bromide

: 501-53-1,94274-21-2
benzyl chloroformate

: 1187201-03-1
1-(2-[allyl(toluene-4-sulfonyl)amino]phenyl)but-3-enylmethyl carbamic acid benzyl ester

Guidance literature:: C₁₈H₂₀N₂O₂S; benzyl chloroformate; In tetrahydrofuran; at 60 ℃; for 1h; Inert atmosphere;

allylzinc bromide; In tetrahydrofuran; at -78 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.tet.2009.05.009

Reference yield: 81.0%

: 1187201-03-1
1-(2-[allyl(toluene-4-sulfonyl)amino]phenyl)but-3-enylmethyl carbamic acid benzyl ester

: N-methyl-[1-(toluene-4-sulfonyl)-1,2,5,6-tetrahydrobenzo[b]azocin-6-yl]carbamic acid benzyl ester

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2009.05.009