(E)-1-Benzenesulfonyl-1-((E)-cyclododec-1-enyl)-4-trimethylsilanyl-but-3-en-2-ol

Base Information

Chemical Name:(E)-1-Benzenesulfonyl-1-((E)-cyclododec-1-enyl)-4-trimethylsilanyl-but-3-en-2-ol
CAS No.:90083-43-5
Molecular Formula:C₂₅H₄₀O₃SSi
Molecular Weight:448.742
Hs Code.:

Synonyms:(E)-1-Benzenesulfonyl-1-((E)-cyclododec-1-enyl)-4-trimethylsilanyl-but-3-en-2-ol

Suppliers and Price of (E)-1-Benzenesulfonyl-1-((E)-cyclododec-1-enyl)-4-trimethylsilanyl-but-3-en-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-Benzenesulfonyl-1-((E)-cyclododec-1-enyl)-4-trimethylsilanyl-but-3-en-2-ol

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Technology Process of (E)-1-Benzenesulfonyl-1-((E)-cyclododec-1-enyl)-4-trimethylsilanyl-but-3-en-2-ol

There total 1 articles about (E)-1-Benzenesulfonyl-1-((E)-cyclododec-1-enyl)-4-trimethylsilanyl-but-3-en-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 58107-34-9,64081-45-4,33755-86-1
(E)-3-trimethylsilyl-2-propenal

: 90083-42-4
(E)-1-Benzenesulfonylmethyl-cyclododecene

: 90083-43-5
(E)-1-Benzenesulfonyl-1-((E)-cyclododec-1-enyl)-4-trimethylsilanyl-but-3-en-2-ol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 ℃;
DOI:10.1021/ja00324a044

Reference yield:

: 90083-43-5
(E)-1-Benzenesulfonyl-1-((E)-cyclododec-1-enyl)-4-trimethylsilanyl-but-3-en-2-ol

: 56975-51-0
15-methylbicyclo<10.3.0>-pentadec-1(12)-en-13-one

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: 65 percent / t-BuOK / 2-methyl-propan-2-ol / 3 h / Ambient temperature; reflux, 36 h

3: 64 percent / H₂SO₄ / acetic acid / 0.17 h / 50 - 60 °C

With sulfuric acid; potassium tert-butylate; In pyridine; acetic acid; tert-butyl alcohol;
DOI:10.1021/ja00324a044