Technology Process of C42H60F13N3O5Si2
There total 4 articles about C42H60F13N3O5Si2 which
guide to synthetic route it.
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synthetic route:
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76598-02-2
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl zinc iodide
- Guidance literature:
-
C34H56IN3O5Si2;
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; α,α,α-trifluorotoluene;
In
tetrahydrofuran;
at 50 ℃;
for 0.0833333h;
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl zinc iodide;
With
copper(l) iodide;
In
tetrahydrofuran;
at 50 - 60 ℃;
for 17h;
DOI:10.1021/jo2015399
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1H-imidazole; dmap / N,N-dimethyl-formamide / 16 h / 20 °C
2.1: pyridine; dmap / 5 h / 35 °C
3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; α,α,α-trifluorotoluene / tetrahydrofuran / 0.08 h / 50 °C
3.2: 17 h / 50 - 60 °C
With
pyridine; 1H-imidazole; dmap; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; α,α,α-trifluorotoluene;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo2015399
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1H-imidazole; dmap / N,N-dimethyl-formamide / 16 h / 20 °C
2.1: pyridine; dmap / 5 h / 35 °C
3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; α,α,α-trifluorotoluene / tetrahydrofuran / 0.08 h / 50 °C
3.2: 17 h / 50 - 60 °C
With
pyridine; 1H-imidazole; dmap; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; α,α,α-trifluorotoluene;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo2015399
