(2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester

Base Information

• Chemical Name: (2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester
• CAS No.: 152830-13-2
• Molecular Formula: C₁₉H₂₃O₅P
• Molecular Weight: 362.362

Synonyms:(2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester

Chemical Property of (2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of (2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester

There total 2 articles about (2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl (S)-Lactate (56777-24-3) → (2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester (152830-13-2)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / tetrahydrofuran / 2 h / 0 °C

2: NaIO₄ / dioxane; H₂O / 3 h / Ambient temperature

With dmap; sodium periodate; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; water;

DOI:10.1021/jm00030a008

Reference yield:

(S)-2-(3-Phenyl-propylphosphinoyloxy)-propionic acid benzyl ester → (2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester (152830-13-2)

Guidance literature:

With sodium periodate; In 1,4-dioxane; water; for 3h; Ambient temperature;

DOI:10.1021/jm00030a008

Reference yield: 97.0%

(2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid benzyl ester (152830-13-2) → (2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid (152830-21-2)

Guidance literature:

With lithium hydroxide; In 1,4-dioxane; for 1h; Ambient temperature;

DOI:10.1021/jm00030a008

upstream raw materials:

benzyl (S)-Lactate

Downstream raw materials:

(2S)-2-(((3-phenylpropyl)hydroxyphosphoryl)oxy)propanoic acid

(S)-5-Methyl-2-oxo-2-(3-phenyl-propyl)-2λ⁵-[1,3,2]dioxaphospholan-4-one

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